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EFFECT NICKEL AND QUENCH-TEMPER PROCESS ON MECHANICAL AND CORROSION PROPERTIES OF ASTM A588 WAETHERING STEEL Rohmah, Miftakhur -; Ramadhan, Gilang; Irawan, Dedi; Utama, Dedi Pria; Romijarso, Toni Bambang
Metalurgi Vol 37, No 3 (2022): Metalurgi Vol. 37 No. 3 Desember 2022
Publisher : National Research and Innovation Agency (BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2540.411 KB) | DOI: 10.14203/metalurgi.v37i3.630

Abstract

The mechanical improvement and "self-protection" properties are mainly needed to develop weather-resistant steel materials. In this study, A588 steel was given thermomechanical treatment (hot-rolling) followed by a quench-tempering process. The A588 is modified by adding 1, 2, and 3 wt% nickel to the primary alloy. Steel is made using a hot rolling process at 750 ℃ for 1 hour with 70% thickness reduction. The sample is heat-treated at 850 ℃ for 1 hour and quenched in water, oil, and open air. The tempering process is conducted at 400 ℃ for 30 minutes. Metallography test is confirmed final microstructural and compared with CCT simulation result. The fast cooling (water and oil quenchant) produces tempered martensite, ferrite, and pearlite, while the air-cooled forms a ferrite-pearlite. The cooling rate significantly affects strength and hardness and the nickel addition on hardness, and both factors have no significant on ductility. The sample owns the highest tensile strength value (~1226 MPa) with 1 %Ni, and the highest ductility value (around 17.1–27.43%) is obtained by air cooling. With 3% Ni, the corrosion rate decreases to 0072 mpy with -432.5 mV for corrosion potential and 0.12µA/cm-2 for current density. 
EFFECT OF COOLING-MEDIUM INDUCED INITIAL STRUCTURE BEFORE INTERCRITICAL ANNEALING ON THE MICROSTRUCTURE AND MECHANICAL PROPERTIES OF LOW ALLOY DUAL-PHASE STEEL Romijarso, Toni Bambang; Rohmah, Miftakhur; Ariati, Myrna; Mabruri, Efendi; Siradj, Eddy Sumarno
Metalurgi Vol 38, No 2 (2023): Metalurgi Vol. 38 No. 2 2023
Publisher : National Research and Innovation Agency (BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/metalurgi.2023.727

Abstract

The present research focused on determining the effect of cooling-medium-induced initial structure before the intercritical annealing induced dual-phase structure in the low alloy steel. Low carbon steel, which consists of containing 0.09 wt.% C was heated at 920 °C for 30 minutes to austenitization and then cooled in various media to provide the different initial structures before the IA (intercritical annealing) process. After austenization, the cooling process in the furnace and open-air provided a ferrite-pearlite phase, while the cooling process in water generated full martensite as the initial structure. Afterwards, the sample was intercritical-annealed at 750 °C (temperature between Ac1 and Ac3 lines or intercritical zone) for 10 minutes and then quenched in water. The water quenching after the austenitizing process improved the mechanical strength of steel (919 MPa), compared to the as-received state (519 MPa) due to martensite formation. As the cooling rate increased after the austenitizing process, the tensile strength increased and the elongation decreased. The different structures before intercritical annealing affected the martensite volume fraction and further correlated with improving mechanical properties. The ferrite and pearlite, as the initial structure before the IA process, provide a smaller fraction of martensite (18.36 vol.% for furnace cooling and 27.85 vol.% for open-air cooling). In contrast, the full martensite as the initial structure before IA generates a higher fraction of martensite (39.25 vol.%). The tensile strengths obtained were 512, 516, and 541 MPa with elongations of 29.8%, 30.1% and 32.6% for cooling furnace, open air and water, respectively. The strain-hardening behavior during the intercritical annealing is not affected by the initial process of the structure.