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MUTTAQIN MUTTAQIN
Universitas Pertamina
Agriculture, Biological Sciences & Forestry Astronomy Automotive Engineering Biochemistry, Genetics & Molecular Biology Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Earth & Planetary Sciences Energy Engineering Immunology & microbiology Mathematics Neuroscience Physics

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SYNTHESIS AND MODIFICATION OF CUPPER 1,4 BENZENEDICARBOXYLATE AS GOOD CANDIDATE FOR POST-COMBUSTION GAS ADSORBENT Muttaqin Muttaqin; Rehan Rizkyta Peranginangin
JURNAL TEKNOLOGIA Vol 4 No 1 (2021): Jurnal Teknologia
Publisher : Aliansi Perguruan Tinggi Badan Usaha Milik Negara (APERTI BUMN)

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

The use of fossil-based fuels has serious implications on the environmental issues because it will increase the emission of carbon dioxide (CO2) gas which will contribute on the global warming. Therefore, it is necessary to develop technologies, methods or materials that can capture or storage CO2 levels in the air. One of the materials that can be used as a CO2 gas absorbent is a material called a metal organic framework (MOF). MOF with a Cu metal core and a ligand, 1,4-benzene dicarboxylic acid will form a porous material with a triclinic crystal structure. This material is called cupper-benzene dicarboxylate (CuBDC). This study aims to synthesize and modify CuBDC with ethylenediamine compound. The characterization results show that CuBDC and CuBDC-modification have been confirmed based on the analysis of Fourier transform infrared spectrophotometer (FTIR) and X-ray diffraction (XRD). The synthesized MOFs have good thermal resistance where the main-frame structure can withstand temperatures up to 300's C. Modified-CuBDC has a much larger surface area, pore diameter and pore volume compared to CuBDC so that modified-CuBDC has the potential to be used as an absorbent material for CO2 gas produced by combustion by the power generation industry or other industries.
A modest method of synthesis Cu- based metal-organic frameworks using benzene dicarbocxylate as a ligan for promising candidate of flue gas CO2 adsorption MUTTAQIN MUTTAQIN; FARID IMAM HIDAYAT
Jurnal Natural Volume 21 Number 3, October 2021
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2011.231 KB) | DOI: 10.24815/jn.v21i3.20035

Abstract

Metal organic framework (MOF) is one of extraordinary materials in many technical field applications. One of them is as CO2 gas adsorbent. We studied, synthesized, and characterized Copper-based material, known as Metal organic frameworks (MOFs), using a solvothermal-based modification method. Copper salt (Cu (NO3)2. 3H2O) and benzene dicarboxylic acid (H2BDC) were mixed and then heated in an oven at 120°C, to produce low impurities, small pore and uniform particle size of materials called CuBDC. Infrared spectroscopy and XRD data confirmed the formation of CuBDC. Furthermore, the result showed that CuBDC frameworks have good thermal stability up to 330°C.  Thereafter SEM picture showed random, layered, and asymmetrical corners structure which is typical of triclinic crystal system. Lastly, specific surface areas and the porosity were analyzed using The Brunauer-Emmett-Teller (BET) method. It recorded 485 m2.g-1 of surface area while average pore volume and average pore size are 0.16 cm3.g-1 and 5.9 Å respectively.   @font-face {font-family:"Cambria Math"; panose-1:2 4 5 3 5 4 6 3 2 4; mso-font-charset:0; mso-generic-font-family:roman; mso-font-pitch:variable; mso-font-signature:-536869121 1107305727 33554432 0 415 0;}p.MsoNormal, li.MsoNormal, div.MsoNormal {mso-style-unhide:no; mso-style-qformat:yes; mso-style-parent:""; margin:0cm; mso-pagination:widow-orphan; font-size:12.0pt; font-family:"Times New Roman",serif; mso-fareast-font-family:"Times New Roman"; mso-ansi-language:EN-US;}.MsoChpDefault {mso-style-type:export-only; mso-default-props:yes; font-size:10.0pt; mso-ansi-font-size:10.0pt; mso-bidi-font-size:10.0pt; mso-ansi-language:IN; mso-fareast-language:IN;}div.WordSection1 {page:WordSection1;}
A modest method of synthesis Cu- based metal-organic frameworks using benzene dicarbocxylate as a ligan for promising candidate of flue gas CO2 adsorption MUTTAQIN MUTTAQIN; FARID IMAM HIDAYAT
Jurnal Natural Volume 21 Number 3, October 2021
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24815/jn.v21i3.20035

Abstract

Metal organic framework (MOF) is one of extraordinary materials in many technical field applications. One of them is as CO2 gas adsorbent. We studied, synthesized, and characterized Copper-based material, known as Metal organic frameworks (MOFs), using a solvothermal-based modification method. Copper salt (Cu (NO3)2. 3H2O) and benzene dicarboxylic acid (H2BDC) were mixed and then heated in an oven at 120°C, to produce low impurities, small pore and uniform particle size of materials called CuBDC. Infrared spectroscopy and XRD data confirmed the formation of CuBDC. Furthermore, the result showed that CuBDC frameworks have good thermal stability up to 330°C.  Thereafter SEM picture showed random, layered, and asymmetrical corners structure which is typical of triclinic crystal system. Lastly, specific surface areas and the porosity were analyzed using The Brunauer-Emmett-Teller (BET) method. It recorded 485 m2.g-1 of surface area while average pore volume and average pore size are 0.16 cm3.g-1 and 5.9 Å respectively.   @font-face {font-family:"Cambria Math"; panose-1:2 4 5 3 5 4 6 3 2 4; mso-font-charset:0; mso-generic-font-family:roman; mso-font-pitch:variable; mso-font-signature:-536869121 1107305727 33554432 0 415 0;}p.MsoNormal, li.MsoNormal, div.MsoNormal {mso-style-unhide:no; mso-style-qformat:yes; mso-style-parent:""; margin:0cm; mso-pagination:widow-orphan; font-size:12.0pt; font-family:"Times New Roman",serif; mso-fareast-font-family:"Times New Roman"; mso-ansi-language:EN-US;}.MsoChpDefault {mso-style-type:export-only; mso-default-props:yes; font-size:10.0pt; mso-ansi-font-size:10.0pt; mso-bidi-font-size:10.0pt; mso-ansi-language:IN; mso-fareast-language:IN;}div.WordSection1 {page:WordSection1;}
Co-Authors FARID IMAM HIDAYAT Rehan Rizkyta Peranginangin