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All Journal Bumi Lestari The Journal of Pure and Applied Chemistry Research
Triyono Triyono
Department of Chemistry, Faculty of Mathematics and Natural Sciences, Gadjah Mada University, Yogyakarta
Agriculture, Biological Sciences & Forestry Humanities Chemical Engineering, Chemistry & Bioengineering Chemistry Earth & Planetary Sciences Energy Environmental Science Materials Science & Nanotechnology Medicine & Pharmacology

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The Chemical Composition and Physical Properties of the Light and Heavy Tar Resulted from Coconut Shell Pyrolysis Uswatun Hasanah; Bambang Setiaji; Triyono Triyono; Chairil Anwar
The Journal of Pure and Applied Chemistry Research Vol 1, No 1 (2012)
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (173.514 KB) | DOI: 10.21776/ub.jpacr.2012.001.01.102

Abstract

The tar resulted from pyrolysis of coconut shell is a waste. It is important to be clarified their chemical composition and physical properties in order to find out their feasibility as source of a fuel. This research was resulted two immiscible organic fractions, and these were further determined their physical properties such as water composition by using ASTM D-95 methods, ash composition (ASTM D-482), flash point C.O.C (ASTM D-92), kinematics of viscosity (ASTM D-445), and caloric valued using bomb calorimetric. In addition, tar composition was determined by gas chromatography-mass spectrometry (GCMS). The result provided oil which was categorized as light and heavy bio-oils. The light bio-oil has specific gravity 0.99, ash content 0.01%, kinematics viscosity 25.5 cSt, flash point <27 oC, pH 3 and heating value 10304 kcal/kg. On the other hand, heavy bio- oils gave specific gravity 1.13, ash 0.46%, kinematics viscosity 185 cSt, flash point 134 oC, pH 2.5 and heating value 6210 kcal/kg. Moreover, the light bio-oil contained 79 compounds which was composed of phenol 16.4%, hydrocarbon 12.4%, phenolic 27.6%, other oxygenated compounds 53.6%, and acetic acid 3%, meanwhile the heavy bio-oils contained of 18 compounds which was consisted of phenol 31.2%, lauric acid 6.0%, phenolic 27.6%, and other oxygenated compounds 35.3%, respectively. With this result, it was clarify that these bio-oils could not be used directly as a fuel for motor nor diesel machinery.
STUDI PENDAHULUAN PEMANFAATAN LIMBAH DESALINASI UNTUK PEMBUATAN Mg/Al HYDROTALCITE-LIKE SEBAGAI ADSORBEN METHYL ORANGE Eddy Heraldy; Dian Prasasti; Karna Wijaya; Sri Juari Santosa; Triyono Triyono
Bumi Lestari Journal of Environment Vol 12 No 1 (2012)
Publisher : Environmental Research Center (PPLH) of Udayana University

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Abstract

The utilization of industrial wastewater into a versatile material that has been the focus of research for economics reasons, environmental and technical. One of the proposed industrial wastewater for a new useful material is wastewater from the desalination process which is also known as brine water. The magnesium content in brine water is able to used as a source of magnesium for the synthesis of Mg/Al hydrotalcite-like compound (Mg/Al HTlc). Mg/Al HTlc are widely investigated for their potential applications in research and industrial processes as adsorbents, catalysts and /or catalyst precursors and pharmaceutical industry excipients. As adsorbents, Mg/Al HTlc are receiving greater interests in the environmental community due to their high adsorption capacity. However, before using natural brine water, has conducted a preliminary study the synthesis of Mg/Al HTlc by using artificial brine water as a model of desalination wastewater. The objective of this research is to synthesis of Mg/Al HTlc from artificial brine water and its ability tested as a methyl orange (MO) adsorbents. The research initiated with the synthesis of Mg/Al HTlc from artificial brine water. Characterization of the Mg/Al HTlc synthesized was confirmed through X-ray Diffraction and FT-IR Spectroscopy. The determination of optimum acidity, adsorption rate, and energy and capacity adsorption were studied. The result showed that pH 3 was the optimum acidity for the adsorption of MO on Mg/Al HTlc. MO was adsorbed at first order adsorption rate of 7.30 × 10-4 s-1 on the Mg/Al HTlc, the adsorption capacity and adsorption energy were 4.36 × 10-5 mol g-1 and 27.54 kJ mol-1, respectively. From the preparatory process and the synthesis of Mg/Al HTlc by using artificial brine water to provide the information that the byproduct of desalination processes (brine water) which are believed to be used for the synthesis of Mg / Al HTlc.
Co-Authors Bambang Setiaji Chairil Anwar Dian Prasasti Eddy Heraldy Karna Wijaya RR. Ella Evrita Hestiandari Sri Juari Santosa