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THE INFLUENCE OF HEAT TREATMENT ON MICROSTRUCTURE AND CORROSION RESISTANCE OF 13Cr-1Mo MARTENSITIC STAINLESS STEEL Siska Prifiharni; Moch. Syaeful Anwar; Efendi Mabruri
Widyariset Vol 2, No 1 (2016): Widyariset
Publisher : Pusbindiklat - LIPI

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1055.684 KB) | DOI: 10.14203/widyariset.2.1.2016.9-16

Abstract

Martensitic stainless steels have been extensively used for a turbine blade. Their properties can be improved in various ways, such as by heat  treatment. This paper aims to investigate the influence of heat treatment on microstructure and corrosion resistance in martensitic stainless steel 13Cr-1Mo. Samples were austenitized at 950 ºC, 1.000 ºC, 1.050 ºC, 1.100 ºC, and tempered at 600 ºC. Austenitized sample at 1.050 ºC was subsequently tempered at 300 ºC, 400 ºC, 500 ºC, 550 ºC, 600 ºC, 650 ºC, and 700 ºC. The tests consist of metallographic observation which was conducted by using an optical microscope and corrosion tests which were conducted by using 3,5% NaCl solution. The results show the evolution of microstructure in martensitic stainless steel 13Cr-1Mo after heat treatment. The microstructure formed consists of tempered martensite, delta ferrite, retained austenite, and carbides. The presence of carbides can also affect corrosion resistance, which will increase along with the increase of tempering temperature due to the increased content of Cr in the carbides. The highest value corrosion resistance was obtained at the austenitizing temperature of 1.050 ºC and tempering temperature of 600 ºC.
THE INFLUENCE OF HEAT TREATMENT ON MICROSTRUCTURE AND CORROSION RESISTANCE OF 13Cr-1Mo MARTENSITIC STAINLESS STEEL Siska Prifiharni; Moch. Syaeful Anwar; Efendi Mabruri
Widyariset Vol 2, No 1 (2016): Widyariset
Publisher : Pusbindiklat - LIPI

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14203/widyariset.2.1.2016.9-16

Abstract

Martensitic stainless steels have been extensively used for a turbine blade. Their properties can be improved in various ways, such as by heat  treatment. This paper aims to investigate the influence of heat treatment on microstructure and corrosion resistance in martensitic stainless steel 13Cr-1Mo. Samples were austenitized at 950 ºC, 1.000 ºC, 1.050 ºC, 1.100 ºC, and tempered at 600 ºC. Austenitized sample at 1.050 ºC was subsequently tempered at 300 ºC, 400 ºC, 500 ºC, 550 ºC, 600 ºC, 650 ºC, and 700 ºC. The tests consist of metallographic observation which was conducted by using an optical microscope and corrosion tests which were conducted by using 3,5% NaCl solution. The results show the evolution of microstructure in martensitic stainless steel 13Cr-1Mo after heat treatment. The microstructure formed consists of tempered martensite, delta ferrite, retained austenite, and carbides. The presence of carbides can also affect corrosion resistance, which will increase along with the increase of tempering temperature due to the increased content of Cr in the carbides. The highest value corrosion resistance was obtained at the austenitizing temperature of 1.050 ºC and tempering temperature of 600 ºC.
Strukturmikro, Kekerasan, dan Ketahanan Korosi Baja Tahan Karat Martensitik 13Cr3Mo3Ni Hasil Quench-Temper dengan Variasi Temperatur dan Waktu Austenisasi [Microstructure, Hardness, and Corrosion Resistant of Martensitic Stainless Steel 13Cr3Mo3Ni after Quench-Temper with Various Austenization Temperature and Time] Siska Prifiharni; Denni Ahmad; Andini Juniarsih; Efendi Mabruri
Metalurgi Vol 32, No 2 (2017): Metalurgi Vol. 32 No. 2 Agustus 2017
Publisher : National Research and Innovation Agency (BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (934.098 KB) | DOI: 10.14203/metalurgi.v32i2.326

Abstract

Martensitic stainless steel type 410 have been extensively used for turbine blade in steam turbine system. Their properties can be improved in various ways, such as modification element and heat treatment. The modified stainless steel in this case is martensitic stainless steel 13Cr-3Mo-3Ni were hot forged then annealed. Afterwards, martensitic stainless steel 13Cr-3Mo-3Ni were prepared and heat treated. Martensitic stainless steel 13Cr-3Mo-3Ni were austenized at temperature 950, 1000, 1050, dan 1100 °C for 1 and 3 hour followed by quench in oil. After quenching, material were tempered at 650°C for 1 hour. Several examinations were carried out on the material such as of hardness test with rockwell C, metallographic using optical microscope, and corrosion test using CMS (corrosion measurement system). The results show that martensitic stainless steel 13Cr3Mo3Ni  at austenitizing temperature of 950 °C for 1 hour and tempering at 650 °C for 1 hour  has the lowest hardness value with hardness value was 33.5 HRC and the lowest corrosion rate 0.02 mpy, whereas  at austenitizing temperature of 1100 °C for 3 hours and tempering at 650 °C for 1 hour has the highest hardness value with hardness value was 46.2 HRC and the highest corrosion rate 1.62 mpy. The microstructures formed are martensite, carbide, and ferrite delta phases. Increased hardness at austenitizing temperature 1100 °C is due to an increase in carbide content in the martensite phase. However, carbide precipitation formed during quenching process can decrease corrosion resistance as Cr and Mo levels decrease in carbides.AbstrakBaja tahan karat martensitik tipe 410 biasa digunakan untuk aplikasi sudu turbin pada steam turbine. Perilaku baja tahan karat jenis ini dapat diperbaiki dengan berbagai cara, salah satunya yaitu dengan cara memodifikasi unsur baja tahan karat tipe 410 tersebut dan perlakuan panas. Baja tahan karat yang telah dimodifikasi dilakukan proses hot forging kemudian dianil. Sampel kemudian dipreparasi dan dilakukan proses perlakuan panas. Proses perlakuan panas yang dilakukan yaitu austenitisasi pada variasi suhu 950, 1000, 1050, dan 1100⁰C selama 1 dan 3 jam dan didinginkan dengan menggunakan media oli. Sampel yang telah diaustenitiasi dilakukan proses temper pada suhu 650⁰C selama 1 jam. Sampel tersebut kemudian dilakukan uji kekerasan, strukturmikro, dan ketahanan korosi yang terjadi setelah melalui proses perlakuan panas. Hasil menunjukkan bahwa nilai kekerasan dan laju korosi yang paling rendah pada suhu austenitisasi 950⁰C selama 1 jam dan paling tinggi pada suhu austenitisasi 1100⁰C selama 3 jam. Hal ini dapat terjadi karena adanya perubahan struktur martensit yang menjadi lebih kasar pada suhu austenitisasi yang lebih tinggi.