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Study of Reduced Graphene Oxide addition on the Electrical Conductivity and Flexural Strength of Metakaolin-based Geopolymer Elsy Rahimi Chaldun; Andrie Harmaji; Nindya Kirana Prabaswari; Lina Nur Listiyowati; Achmad Subhan; Syoni Soepriyanto
Jurnal Keramik dan Gelas Indonesia Vol 29, No 1 (2020): Jurnal Keramik dan Gelas Indonesia
Publisher : Balai Besar Keramik

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32537/jkgi.v29i1.6048

Abstract

Geopolymer with reduced Graphene Oxide (rGO) composite obtanined through Hummers method. This material is a substitute option for graphene because the nature of rGO is easier to produce in large quantities. In theory, it is expected that rGO can increase the flexural strength and electrical conductivity of geopolymer. The rGO composition used varies from 0-1 wt%. Geopolymer and their constituents were characterized by the Three Point Bending, EIS, SEM, FTIR, XRD, and XRF tests. Fly ash-based geopolymers have a flexural strength of 5.2 MPa at a composition of 0.5 wt% rGO, while metakaolin-based geopolymers with an addition of 0.25% rGO produce the highest flexural strength of 5.53 MPa. A frequency of 100,000 Hz tends to facilitate greater electrical conductivity, on fly ash-based geopolymers found electrical conductivity of 5.08 x 10-3 S / m, while for metakaolin-based geopolymers the electrical conductivity is higher ie 1.01 x 10-1 S / m. 
Study of Reduced Graphene Oxide addition on the Electrical Conductivity and Flexural Strength of Metakaolin-based Geopolymer Elsy Rahimi Chaldun; Andrie Harmaji; Nindya Kirana Prabaswari; Lina Nur Listiyowati; Achmad Subhan; Syoni Soepriyanto
Jurnal Keramik dan Gelas Indonesia Vol 29, No 1 (2020): Jurnal Keramik dan Gelas Indonesia
Publisher : Balai Besar Keramik

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32537/jkgi.v29i1.6048

Abstract

Geopolymer with reduced Graphene Oxide (rGO) composite obtanined through Hummers method. This material is a substitute option for graphene because the nature of rGO is easier to produce in large quantities. In theory, it is expected that rGO can increase the flexural strength and electrical conductivity of geopolymer. The rGO composition used varies from 0-1 wt%. Geopolymer and their constituents were characterized by the Three Point Bending, EIS, SEM, FTIR, XRD, and XRF tests. Fly ash-based geopolymers have a flexural strength of 5.2 MPa at a composition of 0.5 wt% rGO, while metakaolin-based geopolymers with an addition of 0.25% rGO produce the highest flexural strength of 5.53 MPa. A frequency of 100,000 Hz tends to facilitate greater electrical conductivity, on fly ash-based geopolymers found electrical conductivity of 5.08 x 10-3 S / m, while for metakaolin-based geopolymers the electrical conductivity is higher ie 1.01 x 10-1 S / m. 
Synthesis and Electrochemical Characterization of Sodium-Ion Battery Anode Carbon Biomassa Based on Sunflower Seed Husk (Helianthus annuus) Simanjuntak, Renaldo; Dinda Amilia; Syahrul Humaidi; Achmad Subhan
Journal of Technomaterial Physics Vol. 5 No. 2 (2023): Journal of Technomaterial Physics
Publisher : Talenta Publisher

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jotp.v5i2.12394

Abstract

This study aimed to synthesize materials from the carbon biomass of sunflower seed husk (Helianthus Annuus) for sodium ion battery anode. A simple carbonization process was carried out by roasting. The chemical activation process was conducted by adding KOH as much as 4M in 100 mL water solution for 20 hours. Then drying was done in the oven at a temperature of 100ºC for 20 hours, and then continued with the sintering process at a temperature of 900ºC for 2 hours. The sintered results were washed and hydrothermal for 20 hours at 200ºC with 4 mL H2O2 and 1 mL EG in 50 mL Teflon. The resulting acid degree was neutralized (pH ~ 7) with distilled water and then dried at 100ºC for 20 hours. The hydrothermal powder was pulverized using a mortar and pestle and then sieved on a 325 mesh sieve. Anode sheets were prepared by mixing active ingredients: PVDF: Super-P with a composition of 85: 10: 5 by adding 2 ml of DMAC solvent. Electrochemical characterization testing was carried out to see the resulting performance—the results obtained from EIS, CV, and CD show that commercial hard carbon is better.