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Leni Widiarti
Universitas Sumatera Utara
Chemistry

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SIFAT TERMAL DAN KELARUTAN DARI CYCLIC LIQUID NATURAL RUBBER Leni Widiarti; Basuki Wirjosentono; Eddyanto Eddyanto
JURNAL KIMIA MULAWARMAN Vol 14 No 2 (2017)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Abstract

Cyclic Liquid Natural Rubber (CLNR) is a cyclical natural rubber which has decreased molecular weight. Synthesis of Cyclic Liquid Natural Rubber (CLNR) can be done in a way that degradation after cyclization. Degradation after cyclization using Cyclic raw material Natural rubber (CNR), the degradation is done by using phenylhydrazine reagents with oxygen gas atmosphere with a flow rate of 2 LMenit-1 for 24 hours. CNR and CLNR thermal analysis by DSC, Tg results obtained amounted to 102.82 ° C and 103.67 ° C, Tc amounted to 362.45 ° C and 330.29 ° C and Tm mounted to 509.24 ° C and 440 , 00 oC. Of CNR and CLNR solubility test has a polarity index of 2.4 to 4.4 and from 2.4 to 4.4.
ANALISIS SIFAT TERMAL DAN UJI KELARUTAN DARI KARET ALAM SIKLIS DAN KARET ALAM CAIR SIKLIS Leni Widiarti; Basuki Wirjosentono; Eddyanto Eddyanto
JURNAL KIMIA MULAWARMAN Vol 16 No 1 (2018)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/jkm.v16i1.481

Abstract

Abstract. The research has done analysis of thermal properties and solubility test of Cyclic Natural Rubber (CNR) and Cyclic Liquid Natural Rubber (CLNR). Cyclic Liquid Natural Rubber (CLNR) is a cyclical natural rubber which has decreased molecular weight. Synthesis of Cyclic Liquid Natural Rubber (CLNR) do by oxidative degradation after cyclic. Oxidative degradation after cyclic using Cyclic Natural Rubber (CNR) and phenylhydrazine reagent with flow rate 2 LMin-1 of oxygen atmosphere during 24 hours. Thermal analysis of Cyclic Natural Rubber (CNR) and Cyclic Liquid Natural Rubber (CLNR) by Differential Scanning Calorimetry (DSC),the glass transition temperature (Tg) of Cyclic Natural Rubber (CNR) and Cyclic Liquid Natural Rubber (CLNR) are 102,82 o C and 103,67 o C, the crystal transition temperature (Tc) of Cyclic Natural Rubber (CNR) and Cyclic Liquid Natural Rubber (CLNR) are 362,45 o C and 330,29 o C and the melting transition temperature ( Tm) of Cyclic Natural Rubber (CNR) and Cyclic Liquid Natural Rubber (CLNR) are 509,24 o C and 440,00 o C. Solubility test by dilute Cyclic Natural Rubber (CNR) and Cyclic Liquid Natural Rubber (CLNR) in some solvent with different properties and polarity index. Solubility test shows the results Cyclic Natural Rubber (CNR) and Cyclic Liquid Natural Rubber (CLNR) has polarity index around 2,4 – 4,4 and 2,4 and 4,4. Keywords: CLNR, CNR, oxidative degradation
Co-Authors Basuki Wirjosentono BASUKI WIRJOSENTONO Eddyanto Eddyanto Eddyanto Eddyanto