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Kinetics of Starch Degradation during Extrusion Cooking of Steady State Flow Konjac (Amorphophallus oncophyllus) Tuber Flour in a Single Screw Extruder Andri Cahyo Kumoro; Diah Susetyo Retnowati; Ratnawati Ratnawati
Bulletin of Chemical Reaction Engineering & Catalysis 2020: BCREC Volume 15 Issue 2 Year 2020 (August 2020)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.15.2.8125.591-602

The presence of glucomannan in Konjac (Amorphophallus oncophyllus) tuber flour has promoted its various applications, especially in the food, drink, drug delivery and cosmetics. Starch is the main impurity of Konjac tuber flour. Although the common wet refining method may result in a high purity Konjac tuber flour, it is very tedious, time consuming and costly. This research aimed to study the kinetics of starch degradation in the extrusion cooking process of dry refining method to produce high quality Konjac tuber flour. In this research, Konjac tuber flour with 20% (w/w) moisture was extruded in a single screw extruder by varying screw speeds (50, 75, 100, 125, 150 and 175 rpm) and barrel temperatures (353, 373, 393, 413 and 433 K). The results showed that the starch extrusion cooking obeys the first reaction order. The reaction rate constant could be satisfactorily fitted by Arrhenius correlation with total activation energy of 6191 J.mol−1 and pre-exponential factor of 2.8728×10−1 s−1. Accordingly, thermal degradation was found to be the primary cause of starch degradation, which shared more than 99% of the energy used for starch degradation. Based on mass Biot number and Thiele modulus evaluations, chemical reaction was the controlling mechanism of the process. The results of this research offer potential application in Konjac tuber flour refining process to obtain high quality flour product. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

Modifikasi Pati Ketela Pohon Secara Kimia dengan Oleoresin dari Minyak Jahe Diah Susetyo Retnowati; Andre Cahyo Kumoro; Sri Budiyati
Jurnal Rekayasa Proses Vol 4, No 1 (2010)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.568

Modifikasi pati akhir-akhir ini banyak dikembangkan dan dipakai untuk keperluan industri makanan, kertas dan tekstil. Modifikasi pati, khususnya secara kimia dilakukan untuk memperbaiki sifat-sifat fungsional pati, terutama jika untuk keperluan bahan dasar makanan. Modifikasi pati ketela pohon dilakukan dengan mereaksikan suspensi pati dengan minyak jahe yang mengandung zat aktif gingerol pada suhu kamar. Hasil percobaan modifikasi menunjukkan bahwa meningkatnya perbandingan antara pati/air/minyak jahe (b/v/v), menghasilkan pati termodifikasi dengan swelling power, kelarutan dan kerapatan cross-link yang lebih tinggi. Pada komposisi pati terhadap air dan minyak jahe, 300:400:0,4 (b/v/v) menghasilkan pati termodifikasi yang cocok digunakan sebagai bahan pengemas makanan yang dapat dimakan (edible food packaging) dengan nilai swelling power, kelarutan dan kerapatan cross-link adalah 7,3 kali; 6,662 mg/mL dan 780,69 rantai/cm3. Sedangkan komposisi pati:air:miyak jahe sebesar 300:300:0,3 (b/v/v) merupakan komposisi terbaik untuk menghasilkan pati termodifikasi sebagai bahan pangan dengan nilai swelling power, kelarutan dan kerapatan cross-link berturut-turut adalah 8,96 kali; 10,55 mg/mL, 203,85 rantai/cm3. Hasil analisis dengan scanning electron microscopy (SEM) menunjukkan bahwa modifikasi pati ketela pohon dengan teknik cross-linking ternyata tidak mengubah struktur permukaan butir pati. Kata kunci: reaksi suspensi, pati ketela pohon, gingerol, swelling power, cross-link Recently, starch modifications have been developed and are applied for food, paper and textile industries. In general, chemical modification has been done to improve starch functionality, especially for bread, cake and snack making. In the present work, suspension method was used to modify cassava starch by gingerol of crude ginger rhizome extract at room temperature. The effect of starch/water/gingerol (w/v/v) ratio on swelling power, water solubility, and cross-link density of the modified starch was investigated. In addition, scanning electron microscopy (SEM) analysis were also conducted to observe possible structural changes of the resulting starch. The experimental results showed that reactant composition that had a starch/water/gingerol (w/v/v) ratio of 300:400:0.4 produced modified starch suitable for edible coating with swelling power of 7.3 times, solubility of 6.662 mg/mL and cross-link density of 780.69 chains/cm3. Meanwhile, reactant having starch/water/gingerol (w/v/v) ratio of 300:300:0.3 produced modified starch that could be used for food with swelling power, solubility and cross-linking density of 8.96, 10.55 mg/mL and 203.85 chains/cm2, respectively. The cross-link densities achieved in this modification process were high and reproducible that indicated a strong interaction between starch and gingerol molecules in water as dispersant. However, there were no noticeable changes found from the micrograph of the SEM analysis on the external surface of the cassava starch. Keywords: suspension method, cassava starch, gingerol, swelling power, cross-link

Extraction and Modification of Gum from Cashew Tree Exudates Using Wheat Starch and Glycerine Andri Cahyo Kumoro; Diah Susetyo Retnowati; Catarina Sri Budiyati
Jurnal Rekayasa Proses Vol 4, No 2 (2010)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.1889

Penelitian ini bertujuan untuk mengekstrak getah pohon mete dan memodifikasi sifatnya untuk dapat digunakan sebagai senyawa pembantu proses pengeringan menggantikan fungsi getah Arab. Dengan menggunakan getah mete termodifikasi dari penelitian ini, permasalahan biaya pada proses pengeringan jus buah dengan spray dryer dapat diatasi. Getah pohon mete dipungut dan diendapkan dari larutan hasil penyadapan dengan bantuan etanol sebagai antisolvent. Dalam penelitian ini gliserin dan pati gandum digunakan sebagai bahan tambahan untuk memodifikasi sifat getah. Hasil penelitian menunjukkan bahwa getah pohon mete termodifikasi yang dihasilkan memiliki kualitas yang baik dan kesamaan sifat dengan getah Arab. Kata kunci : getah pohon mete, getah Arab, modifikasi, pati, gliserin The objectives of this research were to extract cashew tree gum (CTG) from cashew tree exudates and to modify it into a new drying aid, which can act as a substitute for Arabic gum. The cost problem faced in the spray drying of fruit juices is expected to be solved with the use of modified CTG as a replacement of Arabic gum. The CTG was extracted and precipitated from its raw cashew exudates solution with the help of ethanol as antisolvent. Glycerine and wheat starch were the additives used in the modification of the gum. The good quality of modified CTG was obtained based on their close similarity to Arabic gum properties. Keywords: CTG, Arabic gum, modification, starch, glycerine

PENGUATAN USAHA MIKRO DAN KECIL KERUPUK KULIT IKAN CAP MANTAP DI MLATIBARU, SEMARANG DALAM UPAYA PENCAPAIAN SUSTAINABLE DEVELOPMENT GOALS (SDGs) Dessy Ariyanti; Bakti Jos; Andri Cahyo Kumoro; Aji Prasetyaningrum; Diah Susetyo Retnowati
Jurnal Pasopati : Pengabdian Masyarakat dan Inovasi Pengembangan Teknologi Vol 4, No 1 (2022)
Publisher : Fakultas Teknik Universitas Diponegoro

Show Abstract | Download Original | Original Source | Check in Google Scholar

Peran usaha mikro, kecil, dan menengah (UMKM) untuk merealisasikan tujuan pembangunan Berkelanjutan (Sustainable Development Goals SDGs) terutama Tujuan 8 yaitu mendukung pertumbuhan ekonomi yang inklusif dan berkelanjutan, tenaga kerja penuh dan produktif dan pekerjaan yang layak bagi semua di Indonesia sangat besar. Salah satu UMK yang berada di daerah Mlati Baru, Kota Semarang adalah UMK Kerupuk Kulit Ikan Cap Mantap. UMK ini didirikan oleh Bapak Afnan Abdul Syaid pada tahun 2015. UMK ini memerlukan pendampingan sehingga dapat lebih berdaya dan berkembang. Tantangan yang dialami oleh UMK Kerupuk Kulit Ikan Cap Mantap ini adalah proses produksi yang masih mengandalkan cuaca, terutama di musim hujan, proses pengeringan kulit ikan basah sulit dilakukan dan waktu yang dibutuhkan menjadi sangat lama. Tantangan yang kedua adalah keterbatasan alat untuk packing sehingga kerupuk menjadi mudah rusak dan turun kualitasnya. Tantangan yang selanjutnya adalah pemasaran yang selama ini hanya dilakukan secara konvensional yaitu dijajakan di beberapa toko oleh-oleh dan supermarket. Pencapaian target tersebut diupayakan dengan berbagai metode dan kegiatan yang telah disusun yaitu survey awal, riset pasar, analisa SWOT, penyusunan strategi penguatan dan pendampingan, dimana Kegiatan-kegiatan tersebut ditargetkan untuk menghasilkan: Data UMK Kerupuk Kulit Ikan Cap Mantap, Data terbaru hasil riset pasar usaha yang serupa, Analisa SWOT dari UMK Kerupuk Kulit Ikan Cap Mantap, Strategi Penguatan Kerupuk Kulit Ikan Cap Mantap. Luaran yang ingin dicapai pada kegiatan ini adalah pengetahuan tepat guna yang dapat diimplementasikan oleh UMK Kerupuk Kulit Ikan Cap Mantap di Mlatibaru, Semarang dalam upaya peningkatan kapasitas produksi dan pemasaran dari produk yang dihasilkan. Kata kunci : UMKM, kerupuk kulit ikan, pemberdayaan

Modifikasi Pati Sorgum menjadi Maltodekstrin secara Enzimatik Dengan Menggunakan Enzim Alfa Amilase dan Gluko Amilase Noer Abyor Handayani; Kristinah Haryani; Diah Susetyo Retnowati
Jurnal Teknologi Pangan Vol 6, No 1 (2022)
Publisher : Program Studi Teknologi Pangan

Sorgum memiliki kandungan pati yang cukup tinggi sehingga dapat digunakan sebagai bahan baku pembuatan maltodekstrin. Maltodekstrin merupakan produk hidrolisis parsial pati yang dibuat dengan penambahan asam atau enzim. Maltodekstrin merupakan campuran dari glukosa, maltosa dan oligosakarida. Selama ini maltodekstrin banyak diproduksi dari pati jagung dan singkong. Tujuan penelitian adalah mengkaji konsentrasi pati (9%, 12%,15%) dan temperatur operasi (65°C, 70°C, 75°C) pada proses hidrolisis terhadap yield, nilai dextrose equivalen (DE), kelarutan, daya kembang, kadar gula pereduksi dan kadar gula total dari maltodekstrin. Hasil penelitian menunjukkan bahwa proses hidrolisa yang relatif baik terjadi pada temperatur 75°C dan konsentrasi pati 9%. Produk hasil hidrolisis (maltodekstrin) tersebut memiliki nilai kadar gula total 21,12%, kadar gula pereduksi 19,2%, kelarutan 8,5%, nilai DE 16,99, dan daya kembang terendah 6,042.

Kinetics of Starch Degradation during Extrusion Cooking of Steady State Flow Konjac (Amorphophallus oncophyllus) Tuber Flour in a Single Screw Extruder Andri Cahyo Kumoro; Diah Susetyo Retnowati; Ratnawati Ratnawati
Bulletin of Chemical Reaction Engineering & Catalysis 2020: BCREC Volume 15 Issue 2 Year 2020 (August 2020)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.15.2.8125.591-602

The presence of glucomannan in Konjac (Amorphophallus oncophyllus) tuber flour has promoted its various applications, especially in the food, drink, drug delivery and cosmetics. Starch is the main impurity of Konjac tuber flour. Although the common wet refining method may result in a high purity Konjac tuber flour, it is very tedious, time consuming and costly. This research aimed to study the kinetics of starch degradation in the extrusion cooking process of dry refining method to produce high quality Konjac tuber flour. In this research, Konjac tuber flour with 20% (w/w) moisture was extruded in a single screw extruder by varying screw speeds (50, 75, 100, 125, 150 and 175 rpm) and barrel temperatures (353, 373, 393, 413 and 433 K). The results showed that the starch extrusion cooking obeys the first reaction order. The reaction rate constant could be satisfactorily fitted by Arrhenius correlation with total activation energy of 6191 J.mol−1 and pre-exponential factor of 2.8728×10−1 s−1. Accordingly, thermal degradation was found to be the primary cause of starch degradation, which shared more than 99% of the energy used for starch degradation. Based on mass Biot number and Thiele modulus evaluations, chemical reaction was the controlling mechanism of the process. The results of this research offer potential application in Konjac tuber flour refining process to obtain high quality flour product. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

Anaerobic Fermentation of Mixed Fruits Peel Waste for Functional Enzymes Production Employing Palm Sugar and Molasses as The Carbon Source Retnowati, Diah Susetyo; Kumoro, Andri Cahyo; Haryani, Kristinah
Reaktor Volume 23 No.2 August 2023
Publisher : Department of Chemical Engineering, Faculty of Engineering, Universitas Diponegoro

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/reaktor.23.2.71-76

The daily abundant generation of fruit peel waste potentially triggers environmental problems if no appropriate management is performed. Besides, fruit peel waste can be a valuable source for functional enzyme production. This study aims to investigate the use of molasses and palm sugar as sugar source during anaerobic fermentation of banana and papaya peel waste to produce functional enzymes. The fermentation was subjected to biomass at various banana peels to papaya peels mass ratio for 3 months. The feed consisted of sugar:biomass:water, and their mass ratio was kept constant at 1:3:10. Both brown functional enzyme cocktails obtained from the fermentation using palm sugar and molasses as carbon source were acidic with pH of 3.7 and 4.4, respectively. The amylase, protease, and lipase activities of the functional enzyme cocktails was maximum when the biomass mixture contained four portions of banana peel and one portion of papaya peel. In addition, molasses was found to be the better sugar source than palm sugar for producing functional enzymes from aerobic fermentation peel fruits comprises banana and papaya peels. This study proved that fruit peel waste can be converted to valuable functional enzymes as one of the solutions of fruit peel waste management Keywords: anaerobic fermentation; carbon source; enzyme activity; functional enzyme; organic waste

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