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All Journal Jurnal Ilmu-Ilmu Pertanian Indonesia Alotrop Jurnal Pendidikan dan Ilmu Kimia
Nurhamidah Nurhamidah
University of Bengkulu
Agriculture, Biological Sciences & Forestry Chemistry Education

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PENENTUAN KONDISI OPTIMUM HPLC UNTUK PEMISAHAN RESIDU PESTISIDA IMIDAKLOPRID, PROFENOFOS DAN DELTAMETRIN PADA CABAI (Capsicumannum ) Nurhamidah Nurhamidah
Jurnal Ilmu-Ilmu Pertanian Indonesia Vol 7, No 2 (2005)
Publisher : Program Studi Ilmu Tanah Fakultas Pertanian UNIB

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31186/jipi.7.2.87-93

Abstract

The research aim was to determine the optimum ratio and flow rate of mobile phase of acetonitrile: water for separation of pesticide residue of imidacloprid, profenofos and deltamethrin simultaneously with HPLC. The compromise wavelength of the three of residues was measured with UV–VIS spectrophotometer. The ratio of acetonitrile:water consisted of 70 : 30, 60 : 40, 50 : 50, 40 : 60 and 30 : 70 v/v, and the flow rate of the mobile phase consisted of 0,5, 0,75 and 1 mL minutes-1, respectively. The results show the optimum mobile phase was achieved at a ratio of 60:40 v/v and at a wavelength of 270 nm with retention tim of imidacloprid, profenofos and deltamethrin components achieved at 3.0, 6.2 and 17.1 minutes, respectively. The higher ratio of acetonitrile: water and higher mobile phase resulted in accelerating its retention time and a good separation of imidacloprid was not achieved. An unstatisfied separation was also obtained when smaller ratio of acetonitrile: water and lower mobile phase was used. It occurred due to higher deltametrin retention time. 
BIOSINTESIS NANOPARTIKEL PERAK MENGGUNAKAN EKSTRAK BUAH Passiflora flavicarva (MARKISA) UNTUK MENDETEKSI LOGAM BERAT Dina Maryani; M. Lutfi Firdaus; Nurhamidah Nurhamidah
ALOTROP Vol 1, No 1 (2017)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v1i1.2717

Abstract

The aim of this research was to synthesize silver nanoparticle (NPP) by using Passiflora flavicarva (Markisa) fruit extract as detector of heavy metal. The NPP particles produced were determined by their optimum condition on the ratio of the volume of  Passiflora flavicarva passion fruit extract to AgNO3 and the reaction time. The silver nanoparticles produced under optimum conditions will be tested for selectivity against several metals that are often present in the environment, once the selective metal is known then it can be sensitized to the metal using a UV-Vis spectrophotometer to determine the minimal concentrations that can be detected by the silver nanoparticles Formed. The results showed that Passiflora flavicarva passion fruit extracts could be used for the biosynthesis of  NPP particles because they contain vitamin C and flavonoids capable of reducing Ag+ to Ag0 in the form of NPP. The optimal conditions for forming NPP particles are in the 1: 2 ratio with a 2 hour reaction time. From the results of selectivity test of NPP to some heavy metals that often exist in environment, it is known that NPP selective to mercury metal. It was found that selective mercury was followed by a sensitivity test with a UV-Vis spectrophotometer, with sensitive NPP  up to a concentration of 6.7 ppm. From the results of this study it can be concluded that NPP particles formed can be used to detect mercury metal up to a minimum concentration of 6.7 ppm.
PEMANFAATAN ARANG AKTIF SABUT KELAPA SAWIT SEBAGAI ADSOBEN ZAT WARNA SINTETIS REACTIVE RED-120 DAN DIRECT GREEN -26 Melfi Puspita; M. Lutfi Firdaus; Nurhamidah Nurhamidah
ALOTROP Vol 1, No 1 (2017)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v1i1.2727

Abstract

The problem of environmental polution caused by waste of batik industry lately is increasing, so it needed a method to overcome that problem. The aim of this study was to determine the ability of activated charcoal from coconut fiber palm in adsorbing Reactive Red-120 and Direct Green-26 dyes in waste of batik along with determining the parameters of isotherms adsorption using UV-Vis Spectrophotometer analysis method. Variations of pH, contact time, adsorbent weight and temperature were carried out as variable to obtain optimum conditions of the adsorption process. The optimum of conditions for Reactive Red-120  occured at pH 3 and a contact time of 30 minutes, while Direct Green-26  occurred at pH 4 and a contact time of 40 minutes, with each adsorbent weight 150 mg and the temperature 30 °C. Adsorption isotherms determined by Freundlich and Langmuir models with maximum adsorption capacity (Qmax) were obtained for the Reactive Red-120  was 400 mg/g, while Direct Green-26 is 169 mg/g. 
UJI AKTIVITAS ANTIPLASMODIUM FRAKSI N-HEKSANA DAUN Peronema canescens TERHADAP Mus musculus Fenny Andriani; Agus Sundaryono; Nurhamidah Nurhamidah
ALOTROP Vol 1, No 1 (2017)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v1i1.2712

Abstract

Peronema canescens (Sungkai) has been used in Bengkulu as raw herbal remedy to reduce the fever, some people are using as a malaria drug. P.  canescens leaves contain alkaloids, flavonoids, tannins and terpenoids – steroids .This study aims to analyze the effect of P.  canescens leaves  n-hexane fraction.  against paracetemias in Mus musculus infected with Plasmodium berghei, then to prove whether the . P.  canescens leaves n-hexane fraction  has potential as alternative medicine for malaria .   To make P. canescens extract , leaves was macerated using EtOH (96%), then filtrate was evaporated using a rotary evaporator, then fractionated with n-hexane. The 25 healthy  M.musculus  weighing 20-40g each, infected with P.berghei, grouped into 5 ie group 1 (K-) was treated orally with aquades, group 2 (K +) was treated orally with 0.42 mg of Chloroquine, Group 3 (P1) Group 4 (P2), group 5 (P3) was treated orally with a P.  canescens leaves n-hexane fraction  each at a dose of 0.028 ,  0.056 and 0.084 g / kgBW. After 3 days of digestion for each treatment, the amount of erythrocytes was calculated under a microscope. : The giving of the with dose 0,028 g / kgBW able to inhibit paracetemia 33,49%,  0,056 g / kgBW able to  57.91% and  0,084 g / kgBW able to  61.69%   The conclusion is the P. canescens leaves n-hexane fraction  at a dose of 0.028 , 0.056 , and 0.084 g / kgBW orally wil be decreased the amount of paracetemia in M.musculus, and the higher the dose given the higher percent of the inhibition.
UJI AKTIVITAS ANTIOKSIDAN DAN ANTIBAKTERI EKSTRAK DAUN Ricinus communis L (JARAK KEPYAR) Julia Sarfina; Nurhamidah Nurhamidah; Dewi Handayani
ALOTROP Vol 1, No 1 (2017)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v1i1.2725

Abstract

This study aims to determine the antioxidant activity of jarak kepyar’s  leaf extracts (Ricinus communis L.) and to determine of the fraction the growth of Erwinia carotovora. Jarak kepyar’s leaf extracted by maceration method using ethanol and fractionated using n-hexane and ethyl acetate. Antioxidant test using DPPH (1,1-diphenyl-2-picrylhydrazyl) with various concentrations of 125 ppm, 100 ppm, 75 ppm, 50 ppm, 25 ppm, 15 ppm and 5 ppm. Antibacterial test conducted on the active fractions as antioxidants using paper disc method and variations in the concentration of 1000 ppm, 500 ppm, 250 ppm, 125 ppm, 62.5 ppm. Phytochemical test results jarak kepyar’s leaf contain secondary metabolites are alkaloids, flavonoids, phenols and terpenoids. The test results demonstrate the antioxidant activity of ethyl acetate fraction is very strong as an antioxidant with IC50 values of 5.4 ppm and a strong ethanol fraction categorized as antioxidants IC50 of 99.8 ppm. Antibacterial test results showed inhibition of the leaf fraction of  jarak kepyar’s (Ricinus communis L.) against Erwinia carotovora categorized weak growth in ethanol fractions with inhibition zone diameter of 4 mm and being in ethyl acetate fraction with a diameter of 5 mm
AKTIVITAS ANTIOKSIDAN DAN ANTIBAKTERI EKSTRAK DAUN Jatropha gossypifolia L Nia Sapitri Pangestu; Nurhamidah Nurhamidah; Elvinawati Elvinawati
ALOTROP Vol 1, No 1 (2017)
Publisher : University of Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33369/atp.v1i1.2707

Abstract

This study was conducted to determine the activity of Jatropha gossypifolia L (jarak merah’s) leaf extract as an antioxidant and antibactery against acne causing bacteria (Propionibacterium acnes). To obtain an J. gossypifolia L jarak merah’s leaf extract by maceration using 96% ethanol, and then fractionated with n-hexane and ethyl acetate. Testing of antioxidant activity by DPPH method and antibactery activity test by the paper disc method. Antioxidant activity test has done for ethanol fraction, ethyl acetate fraction and n-hexane fraction, while testing for antibacterial activity performed on fractions active as antioxidant. The test results demonstrate the antioxidant activity of ethyl acetate fraction and the ethanol fraction as a fraction very strong with IC50 value of 22.33 ppm for ethyl acetate fraction and 41.04 ppm for ethanol fraction. Then the fraction of ethyl acetate and ethanol fraction antibactery activity test, the result is known that both factions have the ability to inhibit the growth of bacteria Propionibacterium acnes demonstrated by the inhibition zone is formed. In 1000 ppm is formed diameter of the greatest inhibition zone that is equal to 6 mm for ethyl acetate fraction and 5 mm for ethanol fraction.
Co-Authors Budiyanto Budiyanto Dewi Handayani Dina Maryani Elvinawati Elvinawati Fenny Andriani Julia Sarfina M. Lutfi Firdaus M. Lutfi Firdaus Melfi Puspita Nia Sapitri Pangestu