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Titik Pujiati
Chemical Engineering Department, Universitas Muhammadiyah Surakarta, Jl. A. Yani Tromol Pos, Pabelan, Kartasura, Surakarta 57102
Chemical Engineering, Chemistry & Bioengineering Chemistry

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Synthesis of Solid Acid Catalyst from Fly Ash for Eugenol Esterification Nur Hidayati; Titik Pujiati; Elfrida B. Prihandini; Herry Purnama
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 3 Year 2019 (December 2019)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2487.394 KB) | DOI: 10.9767/bcrec.14.3.4254.683-688

Abstract

A series of fly ash-based heterogeneous acid catalysts were prepared by chemical and thermal treatment. Fly ash was chemically activated using sulfuric acid and followed by thermal activation. Characterization methods of XRD, BET, SEM-EDX, and the performance in esterification of eugenyl acetate production was carried out to reveal the physical and chemical characteristics of prepared catalysts. Activated catalyst showed high silica content (96.5%) and high BET surface area of 70 m2.g-1. The catalyst was proven to be highly active solid acid catalyst for liquid phase esterification of eugenol with acetic acid yielding eugenyl acetate. A yield of 43-48% was obtained with activated fly ash catalysts for 90 minutes reaction. These catalysts may replace beneficially the conventional homogenous liquid acid to the eco-friendly heterogeneous one. 
Synthesis of Solid Acid Catalyst from Fly Ash for Eugenol Esterification Nur Hidayati; Titik Pujiati; Elfrida B. Prihandini; Herry Purnama
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 3 Year 2019 (December 2019)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.14.3.4254.683-688

Abstract

A series of fly ash-based heterogeneous acid catalysts were prepared by chemical and thermal treatment. Fly ash was chemically activated using sulfuric acid and followed by thermal activation. Characterization methods of XRD, BET, SEM-EDX, and the performance in esterification of eugenyl acetate production was carried out to reveal the physical and chemical characteristics of prepared catalysts. Activated catalyst showed high silica content (96.5%) and high BET surface area of 70 m2.g-1. The catalyst was proven to be highly active solid acid catalyst for liquid phase esterification of eugenol with acetic acid yielding eugenyl acetate. A yield of 43-48% was obtained with activated fly ash catalysts for 90 minutes reaction. These catalysts may replace beneficially the conventional homogenous liquid acid to the eco-friendly heterogeneous one. 
Co-Authors Elfrida B. Prihandini Herry Purnama Nur Hidayati