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Holia Onggo
Research Center for Physics, Indonesian Institute of Sciences Jalan Cisitu No. 21/154 D Bandung
Computer Science & IT

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THE EFFECT OF Pt LOADING ON ELECTROCHEMICAL PERFORMANCE OF CNT-BASED ELECTROCATALYST Yudianti, Rike; Onggo, Holia
Teknologi Indonesia Vol 37, No 3 (2014)
Publisher : LIPI Press

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (16.051 KB) | DOI: 10.14203/jti.v37i3.230

Abstract

Pt loading on CNT surface as electrocatalyst support affects electrochemical performance of electrocatalyst and proton exchange membrane fuel cell stability. In some recent study, Pt-loaded electrocatalyst was a synthesis using poliol method, undergone by controling weight ratio of Pt percursor and CNT in order to find out the importance of appropriate Pt loading and configuration on electrochemical performance. According to the analysis, Pt-loaded electrocatalyst 23.4 and 36.3% show good material properties and electrochemical performance. Electrocatalyst 23.4% Pt loading was selected for preparing low Pt-loaded electrocatalyst layer by screen printing techniques. Nafion ionomer on electrocatalytic film plays an important role to determine the morphological electrocatalyst surface and performance in changing hydrophobicity and electrochemical properties. Nafion ionomer consequently causes reduction on electrochemical properties from 338.6 to 31.6 m2/g whereas the highest electrochemical surface area (ECSA) is achieved by Pt loading 23.4% in average particle size 3.7 nm, corresponding to Pt activity on hydrogen desorption.
PENGARUH PENAMBAHAN POLY(TETRAFLUOROETHYLENE) PADA KARAKTERISTIK KOMPOSIT BACTERIAL CELLULOSE/ MULTI-WALLED CARBON NANOTUBES Onggo, Holia; Yudianti, Rike
Teknologi Indonesia Vol 35, No 1 (2012)
Publisher : LIPI Press

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (16.051 KB) | DOI: 10.14203/jti.v35i1.173

Abstract

In order to obtain new materials as alternative carbon paper, the bacterial cellulose/multi-walled carbon nanotube (BC/MWCNT) composites were made with and without PTFE by helping agarose, via heating process. The effect of PTFE addition on characteristic BC/MWCNT composite have been studied using thermogravimetric analysis (TGA), scanning electron microscopy (SEM) and impedance bridge. The electrically conductivity of BC / MWCNT/ AG composite (without PTFE addition) is 15.1 x 10-2 S/cm (in-plane) and 0.3 x 10-2 S/cm (through plane). Above 150oC, the composite tends to be destroyed leading to electrical conductivity measurements cannot be performed. In the BC/MWCNT/AG/PTFE composite, heating from 150 to 330oC increased electrically conductivityfrom 4.5 to 24.5 x 10-2 S/cm (in-plane) while through-plane electrically conductivity tend to be stable (0.020.03x10-2 S/cm). After heating at 400oC, the composite was seen better thermal stability but the electrically conductivity was decrease because of carbon particles from AG and BC were decomposed and coating of MWCNT. The PTFE addition was not only for increasing the thermal stability but also as coating material of BC/MWCNT composites.
Co-Authors Rike Yudianti