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Suprihatin Suprihatin
Departement of Physics, University of Lampung, Indonesia, 35141
Control & Systems Engineering Electrical & Electronics Engineering Energy Materials Science & Nanotechnology Physics

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Pengaruh Variasi Waktu Sintering Terhadap Pertumbuhan Fase Bahan Superkonduktor BSCCO-2212 dengan Kadar Ca=1,10 Menggunakan Metode Pencampuran Basah Karlina Rahmah; Suprihatin Suprihatin; Pulung Karo Karo
Journal of Energy, Material, and Instrumentation Technology Vol 1 No 1 (2020): Journal Of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (500.906 KB) | DOI: 10.23960/jemit.v1i1.5

Abstract

This research was conducted to determine the effect of sintering time on the formation of the superconducting phase BSCCO-2212 by calculating the level of purity of the phases formed and looking at the microstructure. The variation of sintering time was 10, 20, 30 and 40 hours using the wet mixing method. The sample was calcinated with 800 °C for 10 hours and sintered with 830 °C. The XRD’s characterization result shows a decrease in phase purity with increasing the sintering time. The relative high volume fraction of the BSCCO-2212/ts10 sample is 90,48% while, the lowest volume fraction of BSCCO-2212/tc40 is 50,74%. The relative high orientation degree of BSCCO-2212/ts20 is 18,47% and the lowest orientation degree of BSCCO-2212/ts10 is 8,4%. The SEM’s characterization result shows of all samples have been oriented and have relatively little space between slabs (voids).
Sintesis dan Karakteristik Struktur, Sifat Fisis, dan Sifat Mekanik Komposit Aspal Silika dengan Variasi Komposisi Aspal Silika (20%:80%wt; 15%:85%wt; 10%:90%wt) Enang Widwiyantoro; Simon Sembiring; Syafriadi Syafriadi; Suprihatin Suprihatin
Journal of Energy, Material, and Instrumentation Technology Vol 1 No 2 (2020): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (370.32 KB) | DOI: 10.23960/jemit.v1i2.20

Abstract

Synthesis and characterization of asphalt silica composites with various compositions have been carried out 20%: 80%wt; 15%: 85%wt; 10%: 90%wt. Silica synthesis was carried out using the sol-gel method. The materials used are rice husks, solid asphalt, distilled water, gasoline, NaOH 1,5% and HNO3 10%. This research was conducted for knowing the effect variations composition of asphalt silica on the phase structure, physical, and mechanical properties. The results of characterization asphalt silica composites with X-Ray Diffraction (XRD) obtained nothing change of phase and so that the phase structure still amorphous that consist of amorph silica and amorph carbon. The result of water adsorbent testing obtained that all variation was infest the standard, which was above 10%. The result compressive strength testing obtained the variation 15%:85%wt got the highest value amount 47,55 Mpa.
Pengaruh Variasi Suhu Sintering Menggunakan Metode Pencampuran Basah M. Muntamijayati; Suprihatin Suprihatin; Yanti Yulianti; Simon Sembiring
Journal of Energy, Material, and Instrumentation Technology Vol 1 No 2 (2020): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (569.158 KB) | DOI: 10.23960/jemit.v1i2.29

Abstract

The superconducting material BPSCCO-2212 with doping Pb = 0,2 has been synthesized by the wet mixing method. Calculation is caried out at 800 °C for 10 hours. While sintering is done at 825 °C, 830 °C, 835 °C and 840 °C for 20 hours. The synthesis result were characterized by XRD X-Ray Diffraction) and SEM (Scanning Electron Microscopy). The XRD spectrum analysis results that have been processed using celref, show that in general the samples produced have formed the BPSCCO-2212 phase (indicated the presence of Bi-2212 peaks) and have been oriented (indicated the existence of peaks with h = k = 0, l even number). For the calculation result obtanced the highest volume fraction value at 830 °C sintering temperature with a value FV = 66,97 % and the highest degree of orientation at 825 °C with a value of P = 76,54 %. The results of the SEM photo recorder generally show that the crystals formed are oriented.
Co-Authors Enang Widwiyantoro Karlina Rahmah M. Muntamijayati Pulung Karo-Karo Simon Sembiring Syafriadi Syafriadi Yanti Yulianti