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PENGARUH PELARUT (ETIL BENZENA), PERBANDINGAN STYRENE BUTADIENE RUBBER (SBR) TERHADAP STIREN, DAN JUMLAH INISIATOR (BPO) PADA PEMBUATAN HIGH IMPACT POLYSTYRENE (HIPS) Dwi Wahyuni
Jurnal Teknologi Dirgantara Vol 2, No.2 Desember (2004)
Publisher : National Institute of Aeronautics and Space - LAPAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30536/j.jtd.2004.v2.a800

Abstract

High impact polystyrene (HIPS) is the widely used material now, and also for the aerospace material as a communication instrument system and an electrical insulation. In order to produce HIPS, there are a view method which can be executed. In this case, the research is executed by the copolymerization processes of styrene butadiene rubber (SBR) solution in styrene. Variables which influence to the result properties (HIPS) are the SBR to styrene ratio, the solvent (ethyl benzene), the benzoyl peroxide initiator (BPO). The properties of the product are tensile strength, impact strength, softening point, melting point and the hardness. The result showed that the properties of the HIPS product was near of the HIPS high heat. The optimal processes condition was the solvent to the styrene monomer ratio was 0.05492, the SBR to the styrene ratio was 0.1236 and the BPO to the styrene ratio was 0,0003. The properties of the HIPS product were: the impact strength was (519-1215) N per cm, the tensil strength not more than was 106 N per cm, the elongation was (36-54) percent and the hardness was (65-69) shore A. This properties achieved at the mixing polymerization processes 4 scale in 11-12 hours, the early mixing at 4 scale 1 hours, the cutting chain 2 drops.
PENELITIAN PEMBUATAN POLI METIL METAKRILAT Dwi Wahyuni; Sri Rukmini Dewi
Jurnal Teknologi Dirgantara Vol 1, No.2 Desember(2003)
Publisher : National Institute of Aeronautics and Space - LAPAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30536/j.jtd.2003.v1.a781

Abstract

The poly methyl methacrylate (PMMA) research has been excecuted. Methyl methacrylate is polymerized by the free radical inisiation with the suspension condition using benzoyl peroxyde inisiator, water as a solution and the gelatine stabilizer, in this reseaarch is executed as a standard ratio (part per part:monomer : water : stabilizer = 100 : 350 : (0.1 1) with the inisiator to monomer ratio variation (part per part) are: 0.1 per 50; 0,175 per 50; 0,25 per 50; 0,25 per 50, the temperature variation are : 30 degree C, 45 degree C, 60 degree C and the time polymerization until 320 minutes. The result showed that the optimum monomer polymerizeation was at the inisiator to monomer ratio 0,25 per 50, the temperature at 45 degree C and at the time polymerization until 300 minutes with the monomer conversion was 86 percent. The Infra Red Spectroscopy analyses showed that there are poly methyl methacrylate in the product. The Gas Liquid Chromatography analysis showed the evolution of the monomer (methil methacrylate concetration.