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Yoktan E Buraen
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Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Computer Science & IT Public Health

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Sintesis Senyawa C-2,8,14,20-TETRA-(2,4,5-Trimetoksi)Fenil Kaliks[4] Resorsinarena dari Senyawa 2,4,5-Trimetoksi Benzaldehida Yoktan E Buraen; Pius D Ola; Reinner I Lerrick
Saintek Lahan Kering Vol 2 No 2 (2019): JSLK Desember 2019
Publisher : Fakultas Pertanian, Universitas Timor

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (728.552 KB) | DOI: 10.32938/slk.v2i2.867

Abstract

The synthesis of C-2,8,14,20-tetra-(2,4,5-trimethoxy)phenyl calix[4] resorcinarene from 2,4,5-trimethoxy benzaldehyde has been done. Through isolation of asaron from Timor Genoak (Acorus calamus) followed by its oxidation with K2Cr2O7, the C-2,8,14,20-tetra-(2,4,5-trimethoxy)phenyl calix[4] resorcinarene has, therefore, been accessed over reflux. The asaron has been isolated as 3.05% of yellow oil whilst, the oxidation produced 2,4,5-trimethoxy benzaldehyde with the yield of 49.49%. The C-2,8,14,20-tetra-(2,4,5-trimethoxy) phenyl calix[4]resorcinarene has been yielded as 89.29% of a brown solid.
Co-Authors Pius Dore Ola Reinner Ishaq Lerrick