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All Journal Stigma : Jurnal Matematika dan Ilmu Pengetahuan Alam Unipa
Yanantra Budi Pramana
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Mathematics

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SINTESIS NANOPARTIKEL NIKEL HIDROKSIDA SECARA ELEKTROKIMIA DENGAN PENAMBAHAN NA-SITRAT SEBAGAI AGEN PEREDUKSI Yanantra Budi Pramana
STIGMA: Jurnal Matematika dan Ilmu Pengetahuan Alam Unipa Vol 9 No 01 (2016)
Publisher : FMIPA : Universitas PGRI Adi Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.36456/stigma.vol9.no01.a327

Abstract

Nickel hydroxide nanoparticles have been synthesized electrochemically. The synthesis based on electrolysis system which bare nickels were used for both cathode and anode. The potential applied during electrolysis was from 25 and 55 V. The sodium citrate concentration 0.3 M, was used to study optimal condition of nickel hydroxide nanoparticles formation. UV-Vis spectroscopy, X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM) and Scanning Electron Microscopy (TEM) were used to characterize themicrostructure and morphology of the products. Spherical nanoparticles were obtained by this method. The generated particles are nearly spherical with a mean size 60 nm depending on synthesis condition. Keywords: Nickel hydroxide nanoparticles, electrochemically, high voltage
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