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All Journal Jurnal Teknik Kimia USU

Renita Manurung

Departemen Teknik Kimia, Fakultas Teknik Universitas Sumatera Utara

Author-ID : 4065359

Chemical Engineering, Chemistry & Bioengineering Chemistry Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology

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PEMURNIAN CRUDE GLYCERINE MELALUI PROSES BLEACHING DENGAN MENGGUNAKAN KARBON AKTIF M. Afif Aufari; Sia Robianto; Renita Manurung
Jurnal Teknik Kimia USU Vol. 2 No. 1 (2013): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Crude glycerine is a concentrated liquid that with the glycerin content less than 88%. Crude glycerine has the dye produced by caroten. Caroten or usually called reddish yellow colour pigments cause the palm oil colour to be reddish yellow. Caroten is soluble in oil and fat but not in the water. Colours has a low quality and did not preferred by consumer and must be eliminated. This compound can be eliminated by a absorption process using activated carbon. The using of crude glycerine will further produce the product drugs and cosmetics industries. This research is conducted to study absorbtion of activated carbon to the crude glycerine impurities that causes the raddish yellow colour. This research do by using mesh, weight, and time of stirring with different variated.

PENGARUH KONSENTRASI Li YANG DI-DOPING KE DALAM KATALIS CaO TERHADAP REAKSI TRANSESTERIFIKASI MINYAK SAWIT Muhammad Tarmidzi; Andre Y. Putra; Renita Manurung; Tjahjono Herawan
Jurnal Teknik Kimia USU Vol. 2 No. 3 (2013): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

The development of biodiesel which is derived from Crude Palm Oil (CPO) shows a risingtrend forpetroleum-based energy reserves are running low.Oil palm is the largestplantation commodity in Indonesia, so, it has high potential as raw material of biodiesel.Transesterification is a reaction of producingbiodiesel (methyl ester). Nevertheless, CPO is easy to be degraded byhydrolysis, so, it couldincrease the amount of Free Fatty Acid (FFA) content which hampers transesterification process. As a consequence, there is formation of soaps as side product. Tomaximize the production of biodiesel which is derived frompalm oil that contains of large amount of FFA (low grade CPO) one of the waysis by applying catalyst through doped-process. This research is held togive information about the effect of Li+ion concentration (inLiNO3 form) which is doped to calcium oxide (CaO) to palm oil transesterification with the large amount ofFFA to produce methyl ester, attemperature of 120oC,the ratio of methanol:CPO = 12:1 (mol/mol), catalyst amount 2,5% (w/w) CPO, for 3,5 hours and usespressured reactor. The variable of research is Liconcentration that isdoped to CaO with concentration: 0%, 1% and 4% (w/w) CaO. The parameter test is methyl ester content that is derived from the result of transesterification with GasChromatography (GC) analysis. The research shows that Li+ion that is doped to CaO catalyst could increase the reaction of methyl ester production which is derived from low grade CPO with FFA>3,5 %, in which the finest of Liconcentration that is doped to CaO is 1%, with result of 90,88% methyl ester.

PEMBUATAN SELULOSA ASETAT DARI α -SELULOSA TANDAN KOSONG KELAPA SAWIT M Roganda L Lumban Gaol; Roganda Sitorus; Yanthi S; Indra Surya; Renita Manurung
Jurnal Teknik Kimia USU Vol. 2 No. 3 (2013): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Utilization of empty fruit bunches of oil palm in Indonesia is still very low, so it should be developed further. One of them by researching the manufacture of cellulose acetate from oil palm empty fruit bunches. The process used in this study is the cellanase with α-cellulose materials. Stages reaction is activation, acetylation, hydrolysis, neutralization and drying. Activation in thethree-neck flask with the addition of 50 ml of glacial acetic acid and stirredfor 3 hour,then added 15 ml of acetic acid anhydride as acetylation agent. Acetylation performed with the variation of time, 2, 2.5, 3, 3.5 hours. In the hydrolysis step, add 2 ml of water and5 ml of glacial acetic acid. The reaction lasted for 30 minutes, then added 1 g of sodium acetate for neutralization, neutralization lasts for 5 minutes. Then do the washing up to the smell of acetic acid is lost, and the last stage is the drying is done with a temperature below 50 oC. The resulting products are then analyzed the degree of substitution, melting point, and then carried out FTIR analysis. The results obtained when the optimum conditions for the acetylation reaction is 2.5 - 3 hours.

PENGARUH WAKTU POLIMERISASI PADA PROSES PEMBUATAN POLIESTER DARI ASAM LEMAK SAWIT DISTILAT (ALSD) Ahmad Rozi Tanjung; Ida Ayuningrum; Renita Manurung
Jurnal Teknik Kimia USU Vol. 2 No. 4 (2013): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Palm Fatty Acid Distillate (PFAD) can be used as raw material for synthesis polyester. The aim of this research is to synthesis of polyester and to determine the effect of reaction time on polymerization methyl ester PFAD. The esterification stage was done at temperature 70oC, reactiontime 120 minute, reactant ratio 1:8 (PFAD:methanol), concentration of catalyst (H2SO4) 1% (w/w) PFAD;polymerization stage was done at temperature 126-132°C, concentration ofcatalyst (BF3-diethyl etherate) 9.2 % (w/w), variation of polymerization reaction time3, 4, and 5 hours; and polyesterification stage was done at temperature 175-200 oC,reactant ratios (w/w) 1:1 (polymerized ME : ethylene glycol), reaction time 4 hours and all ofstage was stirred at 150 rpm. The results showed, in the esterification stage wasobtained methyl ester with iodine value 77.29 g I2/100 g, viscosity 6.90 cP,density 859.91 kg/m3 and analysis byusing GC-MS showed that the purity of methyl ester was 82.23% andmolecular weight 267.97 g/mol. Decreasing in iodine value from 77.294 I2 g/100 g to 63.45-61.14 gI2/100 g indicated that the polymerization process had takenplace. In polyesterification stage wasobtained gel polyester, viscous, dark brown colored solid at room temperature with acid value from13.13 to 21.65 mg KOH/g, viscosity from 14.3 to 19.1 P, and molecular weight 995.03 to 1,522.07g/mol which is more suitable for application of modified polyester. Analysis by using GC showed that the purity of polyester is equal to 65.49%.

Co-Authors Ahmad Rozi Tanjung Andre Y. Putra Ida Ayuningrum Indra Surya, Indra M Roganda L Lumban Gaol M. Afif Aufari Muhammad Tarmidzi Roganda Sitorus Sia Robianto Tjahjono Herawan Yanthi S

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