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All Journal Metalurgi Makara Journal of Technology
Pudji Untoro
Pusat Teknologi Bahan Industri Nuklir (PTBIN)-BATAN Kawasan Puspiptek, Serpong 15314, Tangerang Selatan
Chemical Engineering, Chemistry & Bioengineering Civil Engineering, Building, Construction & Architecture Electrical & Electronics Engineering Energy Engineering Materials Science & Nanotechnology Mechanical Engineering

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ULTRASONIC TREATMENT EFFECT ON THE CONSOLIDATION OF Fe-Cr PARTICLE MIXTURES AFTER COMPACTION AND SINTERING PROCESS Silalahi, Marzuki; Untoro, Pudji; Suharno, Bambang; Harjanto, Sri
Metalurgi Vol 29, No 2 (2014): Metalurgi Vol.29 No.2 Agustus 2014
Publisher : Pusat Penelitian Metalurgi dan Material - LIPI

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (449.765 KB) | DOI: 10.14203/metalurgi.v29i2.289

Abstract

ULTRASONIC TREATMENT EFFECT ON THE CONSOLIDATION OF Fe-Cr PARTICLEMIXTURES AFTER COMPACTION AND SINTERING PROCESS. Fe-Cr microalloys which obtained byultrasonic method are the initial cores for the consolidation process. Therefore its facilitate the formation of thehomogeneous bulk of Fe-Cr alloy with a stable phase. In this research, the synthesis of bulk of Fe-Cr alloy fromthe particles mixture of (Fe+Cr) as the ultrasonic treatment results has been carried out. The particlesconsolidation has been carried out through a process of compaction without adding any lubricants and followedby sintering process in the quartz glass capsules by using induction furnace at 1300 °C. Consolidation of mixtureof Fe-Cr particles that have not undergone previous ultrasonic treatment is also made for a comparison. Theinvestigation by using the SEM (scanning electron microscope)- and density measurements method werepreformed on the Fe-Cr green powders compaction. The bulk of Fe-Cr alloys that are produced trough sinteringprocess was observed using SEM-EDS (energy dispersive spectroscopy), XRD (x-ray diffraction), and densitymeasurements method. The bulk of Fe-Cr alloy prepared with ultrasonically treated Fe-Cr microalloy powders,is more homogeneous in composition and has a better phase stability in comparison to Fe-Cr powders preparedwithout the ultrasonic treatment. Production of bulk Fe-Cr alloy in quartz glass capsule during the sinteringprocess has produced Fe-Cr alloy without oxides.
Transmission Electron Microscopy Characterization of High-Temperatur Oxidation of Fe-20Cr-5Al Alloy Prepared by Focused Ion Beam Technique Dani, Mohammad; Untoro, Pudji; Putra, Teguh Yulius Surya Panca; Parikin, Parikin; Mayer, Joachim; Dimyati, Arbi
Makara Journal of Technology Vol. 19, No. 2
Publisher : UI Scholars Hub

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The Focused Ion Beam (FIB) technique was applied for cross section preparation of the oxidized alloy for Transmission Electron Microscopy (TEM) study. Prior to preparation, the specimens of Fe-20Cr-5Al alloy sheet were oxidized in air at 1200 oC for 2 minutes, 10 minutes, 2 hours, and 100 hours. The microstructure and elemental composition of the samples were characterized using TEM equipped with an Energy Dispersive X-Ray Spectroscopy (EDX). The Electron Energy Loss Spectroscopy (EELS) was used to determine of the light elements. The TEM investigation reveals remarkable microstructure evolution of the specimens during oxidation which generally exhibit a typical multi-layer structure. The TEM images, however, can provide detailed description about the phases occur after oxidation such as the Tungsten (W) and the Gallium (Ga) layers on top of the samples obviously formed during FIB preparation, the formation of Al2O3 and Cr2O3 layer, MgAl2O4 spinel, porosity, Zr/Hf/Mg phases or clusters inside the oxide scale. Hence, the FIB technique has been proven to be reliable preparation technique for microstructural and elemental studies of Fe-20Cr-5Al alloy using TEM.
Co-Authors Arbi Dimyati Bambang Suharno Joachim Mayer, Joachim Marzuki Silalahi Mohammad Dani Parikin Parikin Putra, Teguh Yulius Surya Panca Sri Harjanto Teguh Yulius Surya Panca Putra, Teguh Yulius Surya