Joko Triyono
Staf Pengajar Jurusan Teknik Mesin Universitas Sebelas Maret

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Karakterisasi biokomposit sheep hydroxyapatite (sha)/shellac/tepung terigu Izmi Mahfudi; Joko Triyono; Teguh Triyono
Mekanika: Majalah Ilmiah Mekanika Vol 17, No 2 (2018): MEKANIKA: Majalah Ilmiah Mekanika
Publisher : Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/mekanika.v17i2.35125

Abstract

The development of science and technology has led to new inovations in the medical field, especially ortopedic. The aim of those inovations is to find the alternatives of good materials that can replace the broken sturcture of bone tissue. One of the innovations conducted is the characterization of sheep hydroxyapatite biocomposite. This study aims to investigate the mechanical properties of the material Sheep Hydroxyapatite (SHA) / shellac / wheat fluor. Sheep bone powder already gained from the crusher process and meshing into size of 100 and are soaked for 24 hours, then mixed with wheat flour with the ratio 30 : 70 %wt, 40 : 60 %wt, 50 : 50 %wt, 60 : 40 %wt, 70 : 30 %wt. The next step is the forming process and calcination at a temperature of 900oC with a increase of 10 °C/min. Results of X-Ray Diffraction (XRD) shows that the diffraction peak of SHA/shellac/wheat flour is the value of 2θ: 32.0747º, 33.1943º, 32.5338º. The lowest hardness number of SHA/shellac/wheat flour is 2.86 VHN and the highest is 14.80 VHN, also the highest strong pressure number is 0.20 MPa. The result of microscophy at observation using SEM shows Thar the SHA/shellac/wheat flour 50:50 % wt sample has more porosity as.
Karakteristisasi dan Profil Biodegradasi Material Biokomposit Bovine Hidroksiapatit (Bha)/Ampas Kopi/Shellac Taufiq Hidayat; Joko Triyono; Abu Masykur
Mekanika: Majalah Ilmiah Mekanika Vol 17, No 1 (2018): MEKANIKA: Majalah Ilmiah Mekanika
Publisher : Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/mekanika.v17i1.35048

Abstract

The incidence of fractures in Indonesia is quite high so it needs biomaterials in the field of health that is economical and environmentally friendly. Bovine bone waste can be used for grafting, repairing, replenishing or replacing bones and restoring dental tissue. The purpose of this research is to determine whether the content of the coffee grounds and shellac will disappear after the sintering process, and how the effects of coffee grounds on the porosity and degradation rate of BHA biocomposite materials. This research uses heating method of calcination and sintering. Based on the analysis of test data conducted, it was concluded that SEM EDX observation shows the presence of inorganic elements of Ca and P with high intensity and Na, Mg, O and C with low intensity. Observation of XRD diffraction pattern shows 2θ values of the sample according to the standard diffraction pattern of HA JCPDS 9-432. FTIR functional group analysis showed no major peak points other than phosphate functional groups ( ), carbonates ( ) and hydroxyl (OH-). From these three observations indicate that the content of coffee and shellac dregs has disappeared completely when the sintering process and leaving only the content of BHA and the more mixture of coffee dregs used will decrease the density value and increase the number of porus and accelerate the degradation rate.