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All Journal Acta Chimica Asiana
Syarifa Wahidah Al Idrus
Chemistry Education Study Program, University of Mataram, Indonesia

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Synthesis of 5-nitrovanillin in low temperature as cyanide anion sensor R Rahmawati; Syarifa Wahidah Al Idrus; Supriadi Supriadi; Lalu Sulman
Acta Chimica Asiana Vol. 4 No. 1 (2021)
Publisher : The University of Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/aca.v4i1.46

Abstract

In terms of organic sensor, the molecular structure affects a compound's ability to be used as a colorimetric chemosensor. Here, we present a simple synthesis technique for 5-nitrovanillin sensor. It has been successfully synthesized using nitric acid as a source of nitro groups. Dichloromethane DCM was used as a solvent, and the synthesis was carried out at low temperatures (under 5°C). The method produces a good yield. The nitro group attached to the chemosensor plays a role in prolonging the electron delocalization. Its effect is in the process of anion recognition by the chemosensor. The formation of a sensor-analyte complex between the chemosensor and anion produces a color change in the solution