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All Journal Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains JURNAL REKAYASA KIMIA & LINGKUNGAN
Febrina Dwi Putri, Febrina Dwi
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Chemical Engineering, Chemistry & Bioengineering Energy Engineering

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Pembuatan Biodiesel Dari Minyak Sawit Off -Grade Menggunakan katalis CaO Yang Berasal Dari Kulit Telur Melalui Proses Dua Tahap Putri, Febrina Dwi
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 2, No 2 (2015): Wisuda Oktober Tahun 2015
Publisher : Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains

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Abstract

Biodiesel is an alternative the fuel of derived from vegetable oil transesterification reaction with methanol. Off-grade palm is one of the sources of vegetable oils that can be used as raw material for making biodiesel. In the transesterification reaction using a CaO catalyst. CaO obtained from calcined of eggshell at a temperature of 900ºC during 2 hours. This goal of research to produce biodiesel from off-grade palm use a two-stage reaction, study the performance of the CaO catalyst calcined of eggshell on the transesterification reaction, and determine the reaction of temperature influence, mole ratio of oil:methanol, and the concentration of catalyst on the yield of biodiesel transesterification reaction. Esterification is runned at a temperature of 60°C with a mole ratio of oil:methanol 1:12 and use1%wt of catalyst H2SO4. FFA can be lowered from 16.18% to 0.6%. Transesterification conducted with variations mole ratio of oil:methanol 1:7, 1:9, 1:11, catalyst of CaO concentrations are 2%wt, 4%wt, 6%wt, 50ºC, 60ºC, 70ºC of temperature’s reaction and reaction time during 2 hours. Processing of the data conducted by Response Surface Methodology (RSM), while the number of experiments are determined by Central Composite Design (CCD). Yield is resulted in this research are 62.30%-87.41%. Optimums yield is produced at a temperature of 70ºC with a mole ratio of oil:methanol 1:11 and catalyst of CaO 2%wt. Process conditions which significant effect on the yield of biodiesel are the reaction temperature, mole ratio of oil:methanol, and the interaction between temperature with mole ratio of oil:methanol but in the other side, the catalyst concentration does not have a significant influence.Keywords: biodiesel, CaO, off-grade palm oil, rsm, transesterification
Pembuatan Biodiesel Dari Minyak Sawit Off-Grade Menggunakan Katalis CaO Yang Berasal Dari Kulit Telur Melalui Proses Dua Tahap Putri, Febrina Dwi
Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains Vol 2, No 2 (2015): Wisuda Oktober Tahun 2015
Publisher : Jurnal Online Mahasiswa (JOM) Bidang Teknik dan Sains

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Biodiesel is an alternative the fuel of derived from vegetable oil transesterification reaction with methanol. Off-grade palm is one of the sources of vegetable oils that can be used as raw material for making biodiesel. In the transesterification reaction using a CaO catalyst. CaO obtained from calcined of eggshell at a temperature of 900ºC during 2 hours. This goal of research to produce biodiesel from off-grade palm use a two-stage reaction, study the performance of the CaO catalyst calcined of eggshell on the transesterification reaction, and determine the reaction of temperature influence, mole ratio of oil:methanol, and the concentration of catalyst on the yield of biodiesel transesterification reaction. Esterification is runned at a temperature of 60°C with a mole ratio of oil:methanol 1:12 and use1%wt of catalyst H2SO4. FFA can be lowered from 16.18% to 0.6%. Transesterification conducted with variations mole ratio of oil:methanol 1:7, 1:9, 1:11, catalyst of CaO concentrations are 2%wt, 4%wt, 6%wt, 50ºC, 60ºC, 70ºC of temperature’s reaction and reaction time during 2 hours. Processing of the data conducted by Response Surface Methodology (RSM), while the number of experiments are determined by Central Composite Design (CCD). Yield is resulted in this research are 62.30%-87.41%. Optimums yield is produced at a temperature of 70ºC with a mole ratio of oil:methanol 1:11 and catalyst of CaO 2%wt. Process conditions which significant effect on the yield of biodiesel are the reaction temperature, mole ratio of oil:methanol, and the interaction between temperature with mole ratio of oil:methanol but in the other side, the catalyst concentration does not have a significant influence.Keywords: biodiesel, CaO, off-grade palm oil, rsm, transesterification
Pembuatan Biodiesel dari Minyak Sawit Off-Grade Menggunakan Katalis CaO Melalui Proses Dua Tahap Putri, Febrina Dwi; Helwani, Zuchra; Drastinawati, Drastinawati
Jurnal Rekayasa Kimia & Lingkungan Vol 10, No 3 (2015): Jurnal Rekayasa Kimia & Lingkungan
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v10i3.3063

Abstract

Biodiesel merupakan sumber bahan bakar alternatif yang bisa dihasilkan dari minyak nabati melalui transesterifikasi dengan metanol. Sawit Off-grade merupakan salah satu sumber minyak nabati yang mempunyai potensi untuk digunakan sebagai bahan dasar produksi biodiesel. Reaksi transesterifikasi dilangsungkan dengan bantuan katalis CaO dari cangkang telur yang dikalsinasi pada suhu 900C selama 2 jam. Tujuan dari penelitian ini adalah untuk memproduksi biodiesel dari minyak sawit off-grade melalui reaksi dua-tahap, melihat performa katalis Cao terhadap reaksi transesterifikasi, serta mempelajari pengaruh temperatur reaksi, rasio mol minyak:metanol dan konsentrasi katalis terhadap yield biodiesel pada reaksi transesterifikasi. Esterifikasi dilakukan pada suhu 60C dengan perbandingan mol minyak:metanol 1:12 menggunakan 1%wt katalis H2SO4. Asam lemak bebas (ALB) tereduksi dari 16,18% menjadi 0,6%. Reaksi transesterifikasi dilakukan dengan variasi perbandingan mol minyak:metanol 1:7, 1:9, 1:11, konsentrasi katalis 2%wt, 4%wt, 6%wt, serta suhu reaksi pada 50C, 60C, 70C selama 2 jam. Data yang diperoleh diproses dengan menggunakan response surface methodology (RSM), sedangkan jumlah eksperimen ditentukan dengan central composite design (CCD). Yield yang diperoleh pada penelitian ini yaitu sebanyak 62,30%-87,41%. Yield optimum dihasilkan pada reaksi dengan suhu 70C menggunakan minyak:metanol dengan perbandingan 1:11 dan katalis CaO 2%wt. Kondisi proses yang berpengaruh terhadap yield biodiesel adalah suhu reaksi, perbandingan mol minyak:metanol, serta interaksi antara suhu dengan perbandingan mol minyak:metanol. Akan tetapi tidak ditemukan adanya pengaruh signifikan konsentrasi katalis terhadap yield biodiesel.
Co-Authors Drastinawati Drastinawati, Drastinawati Zuchra Helwani, Zuchra