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All Journal Indonesian Journal of Chemistry
Hazim Yahya Al-Gubury
Department of Chemistry, College of Sciences for Women, University of Babylon, Hilla, Iraq
Chemical Engineering, Chemistry & Bioengineering Chemistry

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Synthesis and Characterization of ZnO Nanoparticles via Thermal Decomposition for Zn(II) Schiff Base Complex Hadeer Mohammed Subhi; Ali Taleb Bader; Hazim Yahya Al-Gubury
Indonesian Journal of Chemistry Vol 22, No 5 (2022)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.74753

Abstract

Zinc(II) oxide (ZnO) nanoparticles were easily produced in this research by thermal decomposition of the Zn(II) Schiff base complex. The ligand was synthesized via condensation of benzylamine with 2-hydroxybenzaldehyde. The Zn(II) Schiff base complex was prepared by the reaction between zinc salt and Schiff base with the molar ratio of 1:1 (metal:ligand). The binary complex powder was calcined at 700 °C to produce ZnO nanoparticles. Various methods were used to characterize the Schiff base, complexes, and nanoparticles, including 1H and 13C-NMR, FTIR, TGA, DTA thermal analysis, XRD, TEM, SEM, EDX, BET, UV-Vis Diffuse Reflectance, atomic absorption, melting point, and UV-Vis spectrophotometer. ZnO nanoparticles had an average crystallite size of 48.2 nm.
Co-Authors Ali Taleb Bader Hadeer Mohammed Subhi