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Muqoyyanah Muqoyyanah
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Agriculture, Biological Sciences & Forestry Chemistry Mathematics Physics

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HYDROTHERMAL GROWTH AND SQUEEGEE METHOD IN THE FABRICATION OF MIXED-PHASE TiO2 NANOSTRUCTURES Muqoyyanah Muqoyyanah; Suriani Abu Bakar; Azmi Mohamed; Norhayati Hashim; Mohamad Hafiz Mamat; Mohamad Firdaus Malek; Mohamad Khairul Ahmad
Sainmatika: Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam Vol. 13 No. 2 (2016): Sainmatika : Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam
Publisher : Universitas PGRI Palembang

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (866.309 KB) | DOI: 10.31851/sainmatika.v13i2.966

Abstract

In this work, the modification of TiO2 nanostructures based on its morphology and crystallinity phase were fabricated using a simple method. Hydrothermal growth method was used to synthesize nanorods and nanoflowers, while nanoparticles was applied using squeegee method. The average length and diameter of the as-grown nanorods were 3.5 and 46-215 nm, respectively. Meanwhile, the average total thickness and band gap value of mixed-phase TiO2 nanostructures were 15.98-24.54 nm and 2.84 eV, respectively. Based on its structural and electrical properties, the fabricated film has great potential to be applied as photoanode semiconductor layer for dye-sensitized solar cells application. Key words: TiO2, Nanostructures, Mixed-phase, Hydrothermal, Squeegee
THE USE OF TRIPLE-TAILS CUSTOM-MADE SURFACTANT IN THE PRODUCTION OF GRAPHENE OXIDE THIN FILM AS TRANSPARENT CONDUCTIVE ELECTRODE Muqoyyanah Muqoyyanah; Suriani Abu Bakar; Azmi Mohamed; Norhayati Hashim; Mohamad Hafiz Mamat; Mohamad Firdaus Malek; Mohamad Khairul Ahmad
Sainmatika: Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam Vol. 14 No. 1 (2017): Sainmatika : Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam
Publisher : Universitas PGRI Palembang

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (809.406 KB) | DOI: 10.31851/sainmatika.v14i1.1107

Abstract

In this work, graphene oxide (GO) and reduced GO (rGO) thin films were fabricated from GO and rGO using the custom-made and commercial surfactants, which were sodium 1,4-bis (neopentyloxy)-3-(neopentyloxycarbonyl)-1,4-dioxobutane-2-sulphonate and sodium dodecyl sulphate, respectively. The GO solution was synthesized using electrochemical exfoliation method followed by reduction process utilizing hydrazine hydrate to produce rGO solution. The GO and rGO transfer process were done using spraying deposition method on fluorine-doped tin oxide substrate. The fabricated GO and rGO thin films consists of several layers resulted in high transparency over 85% with maximum transmittance of 93.69%. Based on several characterizations, the fabricated GO and rGO thin films have potential to be applied as transparent conductive electrode.Key words: Custom-made, Surfactant, Electrochemical, Spraying, Electrode. ABSTRAKDalam penelitian ini, film tipis grafin oksida (GO) dan grafin oksida yang direduksi (rGO) difabrikasi dari GO dan rGO menggunakan surfaktan yang dibuat khusus dan surfaktan komersial yaitu secara berurutan adalah sodium 1,4-bis (neopentyloxy)-3-(neopentyloxycarbonyl)-1,4-dioxobutane-2-sulphonate dan sodium dodecyl sulphate. Larutan GO disintesis menggunakan metode eksfoliasi elektrokimia diikuti dengan proses reduksi menggunakan hidrazin hidrat untuk menghasilkan larutan rGO. Proses transfer GO dan RGO dilakukan dengan menggunakan metode deposisi penyemprotan diatas substrat oksida timah oksida dengan doping florin. Film tipis GO dan rGO yang difabrikasi terdiri dari beberapa lapis dengan transparansi tinggi mencapai 85% dengan transmitansi maksimum sebesar 93,69%. Berdasarkan beberapa karakterisasi, film tipis GO dan rGO ini memiliki potensi untuk diaplikasikan sebagai elektroda konduktif transparan.Kata Kunci: dibuat khusus, surfaktan, elektrokimia, penyemprotan, elektroda
THE STRUCTURAL PROPERTIES OF GRAPHENE OXIDE AND REDUCED GRAPHENE OXIDE GROWN ON STAINLESS STEEL SUBSTRATE Kyairi Zaid; Suriani Abu Bakar; Muqoyyanah Muqoyyanah
Sainmatika: Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam Vol. 14 No. 2 (2017): Sainmatika : Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam
Publisher : Universitas PGRI Palembang

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (723.834 KB) | DOI: 10.31851/sainmatika.v14i2.1295

Abstract

In this paper, the structural properties of graphene oxide (GO) and reduced graphene oxide (rGO) based on custom-made, sodium 1,4-bis (neopentyloxy)-3-(neopentyloxycarbonyl)-1,4-dioxobutane-2-sulphonate (TC14) surfactant were investigated. GO was synthesized by electrochemical exfoliation and chemical reduction process utilizing hydrazine hydrate was further done to produce rGO. The obtained GO and rGO solution were then transferred to stainless steel substrate by spraying deposition method. Based on several characterizations, the fabricated film has potential to be used as electrode for water treatment application. Key words: Graphene Oxide, Reduced Graphene Oxide, Stainless Steel, Electrochemical, Spraying. ABSTRAK Dalam artikel ini diteliti sifat struktural dari oksida grafin (GO) dan oksida grafin yang direduksi (rGO) menggunakan surfaktan sodium 1,4-bis (neopentyloxy)-3-(neopentyloxycarbonyl)-1,4-dioxobutane-2-sulphonate (TC14) yang dibuat khusus. GO disintesis menggunakan eksfoliasi elektrokimia dan proses reduksi kimiawi menggunakan hidrazin hidrat untuk menghasilkan rGO. Larutan GO dan rGO yang dihasilkan kemudian ditransfer ke substrat stainless steel degan metode deposisi penyemprotan. Berdasarkan beberapa karakterisasi, film yang difabrikasi memiliki potensi untuk digunakan sebagai elektroda untuk aplikasi pengolahan air. Kata kunci: Oksida grafin, oksida grafin direduksi, stainless steel, elektrokimia, penyemprotan
Co-Authors Azmi Mohamed Kyairi Zaid Mohamad Firdaus Malek Mohamad Hafiz Mamat Mohamad Khairul Ahmad Norhayati Hashim Suriani Abu Bakar