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Nisreen H. Karam
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Medicine & Pharmacology

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Synthesis and Phase Transition Study of New Mesogence Derived from 1, 4-Phenylenediamine Nisreen H. Karam
Journal of Global Pharma Technology Volume 11 Issue 07
Publisher : Journal of Global Pharma Technology

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Abstract

This work include synthesized and characterization the compound [I] by reaction 1,4-phenylenediamine with chloro acetic acid  then this compound  reaction with methanol in present  sulfuric acid to synthesized ester compound [II] after that reaction with hydrazine hydrate to synthesized acide hydrazide [III] and the later compound reaction with substituted acetophenone[IV]n to synthesized substituted acetophenone hydrazones[V-XI]. In addition synthesized4-formylpyrazole derivatives [XII-XVIII] via cyclisation substituted acetophenone hydrazones [V-XI] with Vilsmeier-Haack reagent DMF/POCl3. The compounds characterized by melting points, FTIR, 1HNMR and mass spectroscopy. The mesomorphic behavior studied by using polarized optical microscopy and differential scanning calorimetry. Keywords: Liquid crystals, 4-formylpyrazole, 1, 4-phenylenediamine, Mesomorphic properties.
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