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Iftikhar Ahmed Hussein
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Medicine & Pharmacology

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Synthesis and Characterization of Some New Derivatives Starting from (4, 4'-diaminophenoxy) Ethane Containing Diazonium Groups Iftikhar Ahmed Hussein
Journal of Global Pharma Technology Volume 11 Issue 2: 2019
Publisher : Journal of Global Pharma Technology

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Abstract

The diazonium salts are highly reactive compounds. They are used as intermediate in different reactions. The diazonium salt [C2] was synthesized and reacted upon with (Acetyl acetone, ethyl acetoacetate, salicyladehyde) to produce [C3-C5].Then reacted [C3, C4] with hydrazine hydrate 80% due to [C6,C7]  . Then reacted [C5] with (Methyldopa and Atenolol) as drugs obtained [C8, C9].The prepared derivatives were identified by infrared spectra, 1HNMR, and physical properties.Keywords: Azo compounds, Heterocyclic rings, Schiff bases.
Synthesis and Biological Activities of Some New Derivatives Based on 2-amino-5-mercapto-1, 3, 4-Thiadiazole Containing Imide, β-Lactam Rings Iftikhar Ahmed Hussein
Journal of Global Pharma Technology Volume 11 Issue 03
Publisher : Journal of Global Pharma Technology

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Abstract

New series of 2-amino-5-mercapto-1,3,4-thiadiazole derivatives compounds are synthesized [S1-S4], then converted to Schiff′s base [S5-S10] which is reacted with chloro acetyl chloride due to the existence of  ????-Lactam compound[S11-S16]. The prepared derivatives are identified by infrared spectra studies, 1HNMR, and physical properties. The antibacterial strains have been investigated: an activity has been shown against Gram (+ve) bacterial (stapylococus and Gram (- ve) bacteria (Esherichiacoli).Key words: 1, 3, 4-Thiadiazole, Schiff bases, Heterocyclic rings, Biological activity.
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