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All Journal ALCHEMY Jurnal Penelitian Kimia
Yeni Maulidah Muflihah
Jurusan Kimia, Fakultas MIPA, Universitas Jember, Jember
Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Environmental Science Materials Science & Nanotechnology

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Batch Injection Potentiometry Asam Aspartat, Asam Glutamat dan Arginin Menggunakan Elektroda Tungsten Oksida Yeni Maulidah Muflihah; Heny Masruroh; Zulfikar Zulfikar
ALCHEMY Jurnal Penelitian Kimia Vol 10, No 1 (2014): March
Publisher : UNIVERSITAS SEBELAS MARET (UNS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (259.016 KB) | DOI: 10.20961/alchemy.10.1.18.1-10

Abstract

The presence of aspartic acid, glutamic acid and arginine in solution can be detected by potentiometric method using tungsten oxide electrode in a batch system. Characterization of tungsten oxide electrode used include linear range, limit of detection, sensitivity and reproducibility. Buffer type and concentration effect also studied to optimize the measurement results. Optimum conditions for detecting arginine was at pH 6.0 with a phosphate buffer concentration of 0.5 x 10-3 M. Correlation coefficient was obtained for 0.9864, the detection limit of 5.24 x 10-6 M, sensitivity 16.1 mV/decade with reproducibility 0 –7 %. Glutamic acid has a correlation coefficient of 0.9789, the detection limit of 3.80 x 10-6 M, the sensitivity of 9.2 mV/decade and reproducibility of 0 – 6 %. Aspartic acid has a correlation coefficient of 0.9949, the detection limit of 7.76 x 10-6 M, sensitivity of 13.4 mV/decade and reproducibility of 0 – 5 %.
Co-Authors Heny Masruroh Zulfikar Zulfikar