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Muhammad Romli
Departemen of Agroindustrial Technology, Faculty of Agriculture Engineering and Technology, Bogor Agricultural University, Bogor, Indonesia
Control & Systems Engineering Earth & Planetary Sciences Electrical & Electronics Engineering Energy Engineering

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Synthesis of Trimethylolpropane Esters of Calophyllum Methyl Esters : Effect of Temperature and Molar Ratio Yeti Widyawati; Ani Suryani; Muhammad Romli; Sukardi Sukardi
International Journal of Renewable Energy Development Vol 3, No 3 (2014): October 2014
Publisher : Center of Biomass & Renewable Energy, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/ijred.3.3.188-192

Abstract

Trimethylolpropane esters were synthesized by transesterification of calophyllum methyl esters and trimethylolpropane using a calcium oxide as the catalyst. The results showed that the optimal reaction conditions (temperature: 130 0C, reaction time: 5 h, reactant molar ratio: 3.9:1, catalyst amount 3%w/w, and formed  trimethylolpropane ester of 79.0% were obtained. The basic physicochemical properties of the trimethylolpropane esters were the following : kinematic viscosities of 56.40 cSt and 8.8 cSt at 40 0C and 100 0C,  viscosity index 193, flash point 218 0C and pour point -3 0C. So Methyl esters of fatty acids of would callophylum  methyl ester is good raw material for the synthesis of lubricating oils.
Co-Authors Ani Suryani Sukardi Sukardi Yeti Widyawati