Claim Missing Document
Check
Articles

Found 2 Documents
Search

Green Synthesis and Characterization of Zinc Oxide Nanoparticles using Corchorus olitorius Leaf Extract Kpega, Tyosue Christopher; Habila, James Dama; Okon*, Idongesit Edem; Ekwumemgbo, Patricia Adamma
Aceh International Journal of Science and Technology Vol 12, No 3 (2023): December 2023
Publisher : Graduate School of Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.13170/aijst.12.3.34013

Abstract

Green synthesis of metal oxide nanoparticles has gained prominence in recent years, resulting from the absence of toxic chemicals, low energy requirement, and eco-friendliness. This paper reports the green synthesis of zinc oxide nanoparticles (ZnO-NPs) using plant extract as a reducing agent. The ZnO-NPs were synthesized using Corchorus olitorius leaf extract and zinc acetate dihydrate, Zn (CH3COO)2.2H2O as precursor. The synthesized ZnO-NPs were characterized by the application of UVVis spectroscopy, Transmission Electron Microscopy (TEM), X-ray diffraction (XRD), Energy Dispersive X-ray Spectroscopy (EDX) and Fourier Transform Infrared Spectroscopy (FTIR). UV-vis indicated the reduction of zinc acetate dihydrate into ZnO-NPs by the leave extract. XRD and TEM revealed that the average size of the synthesized ZnO-NPs was 22 nm. The XRD pattern showed the hexagonal wurtzite crystalline nature of the synthesized ZnO-NPs. The elemental composition obtained from EDX showed that the synthesized ZnO-NPs are primarily composed of three elements: Zn (75.20 %), O (20.48.7%), and C (4.32). Examination of stretching and bonding in the ZnO-NPs using FT-IR revealed the presence of Zn-O bonding at 430.37403.93 cm-1.
Assessment of Safety Measures and Operational Challenges of Inland Waterway Transport along Oron - Calabar Route, Nigeria Okon*, Idongesit Edem; Jatau, Solomon Usman; Attah, Anthony Abutu
Aceh International Journal of Science and Technology Vol 12, No 2 (2023): August 2023
Publisher : Graduate School of Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.13170/aijst.12.2.27542

Abstract

This study assessed the safety measures and operational challenges of inland waterway transport along the Oron - Calabar route. Observation and structured questionnaires were used for the collection of data. Quantitative data was analyzed using descriptive statistics, while qualitative data was coded and analyzed using the 4-point Likert scale, which was converted to a relative importance index (R.I.I.) for each factor, posing a challenge to operators. The result showed that safety equipment was provided onboard boats by operators. The R.I.I. computed showed that boat and engine replacement (R.I.I. = 0.874) was the most challenging factor, while water hyacinth (R.I.I. = 0.418) was the least. Other challenges were frequent bad weather conditions, high running costs, floating logs and debris, extortion by law enforcement agents, difficulty making headway against the opposite current, high cost of safety equipment, passengers' refusal to adhere to safety measures, and poor berthing facilities in their order of impact. Proper funding and enforcement of safety measures are hereby recommended.