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All Journal Jurnal Presipitasi : Media Komunikasi dan Pengembangan Teknik Lingkungan Journal of Mathematical and Fundamental Sciences JKPK (Jurnal Kimia dan Pendidikan Kimia) Equilibrium Journal of Chemical Engineering

Purwanto, Agus

Department Of Chemical Engineering, Faculty Of Engineering, Sebelas Maret Universitas, Jl. Ir. Sutami 36A, Surakarta, Central Java 57126

Author-ID : 748852

Agriculture, Biological Sciences & Forestry Astronomy Chemical Engineering, Chemistry & Bioengineering Chemistry Earth & Planetary Sciences Energy Engineering Materials Science & Nanotechnology Mathematics Physics

Published : 7 Documents Claim Missing Document

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Articles

Metal-Organic Frameworks Based on Zinc(II) and Benzene-1,3,5-Tricarboxylate Modified Graphite: Fabrication and Application as an Anode Material in Lithium-Ion Batteries Witri Wahyu Lestari; Wulan Cahya Inayah; Fitria Rahmawati; Larasati Larasati; Agus Purwanto
Journal of Mathematical and Fundamental Sciences Vol. 52 No. 1 (2020)
Publisher : Institute for Research and Community Services (LPPM) ITB

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.math.fund.sci.2020.52.1.6

This research was aimed at synthesizing metal-organic frameworks (MOFs) based on zinc(II) and a benzene-1,3,5-tricarboxylate (BTC) linker in combination with graphite as anode material in lithium-ion batteries. The MOFs were prepared using sonochemical and solvothermal methods, which led to different materials: [Zn3(BTC)2·12H2O] (MOF 1) and [Zn(BTC)·H2O·3DMF] (MOF 2). The produced materials were characterized by powder X-ray diffraction (PXRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), thermogravimetric/differential thermal analysis (TG/DTA), and a battery analyzer. Refinement of the XRD data was performed using the Rietica and Le Bail method. Sharp and intense peaks indicated that the materials had a high degree of crystallinity. The morphology of the materials as analyzed by SEM was cubic, with an average crystal size of 8.377 ± 4.276 µm for MOF 1 and a larger size of 16.351 ± 3.683 µm for MOF 2. MOF 1 was thermally stable up to 378.7 °C while MOF 2 remained stable up to 341.8 °C, as demonstrated by thermogravimetric analysis. The employment of the synthesized materials as anode in a lithium ion battery was proved to yield higher specific capacity and cycle stability compared to those using a graphite anode. The lithium-ion battery with 5 wt% MOF 1 exhibited the highest performance with an efficiency of 97.28%, and charge and discharge specific capacities of 123.792 and 120.421 mAh/g, respectively.

Training of Electric Bike Assembly with Lithium Batteries at SMK Muhammadiyah 6 Karanganyar Tika Paramitha; Endah Retno Dyartanti; Hendri Widiyandari; Arif Jumari; Adrian Nur; Inayati Inayati; Anatta Wahyu Budiman; Agus Purwanto
Equilibrium Journal of Chemical Engineering Vol 5, No 1 (2021): Volume 5, No 1 July 2021
Publisher : Program studi Teknik Kimia UNS

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/equilibrium.v5i1.53965

With the increasing development of the battery and electric vehicle industry, student's and teacher's understanding of lithium batteries and skills in assembling electric bikes are very important in competing for jobs in these fields. Educational activities regarding batteries and training on assembling electric bike are carried out at SMK Muhammadiyah 6 Karanganyar, because there were no facilities that support the learning and teaching process about electric vehicles and batteries. The method used in this training is lecture, discussion and practice method. The material presented was about the technology of making lithium batteries and electric bike components. While practical activities include the stages of converting conventional bikes into electric bikes with energy from lithium batteries. This activity shows that participants can understand batteries and can apply batteries to electric vehicles, especially electric bikes.

Edukasi Teknologi Produksi dan Aplikasi Baterai Lithium Ion pada Kendaraan Listrik di SMK Muhammadiyah 6 Karanganyar Endah Retno Dyartanti; Tika Paramitha; Hendri Widiyandari; Arif Jumari; Adrian Nur; Anatta Wahyu Budiman; Agus Purwanto
Equilibrium Journal of Chemical Engineering Vol 4, No 2 (2020): Volume 4 No 2 December 2020
Publisher : Program studi Teknik Kimia UNS

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/equilibrium.v4i2.45154

Abstrak. Kendaraan listrik merupakan kendaraan yang digerakkan dengan motor listrik dan mendapat sumber daya listrik yang tersimpan dalam baterai. Keuntungan penggunaan kendaraan listrik dibandingkan dengan kendaraan konvesional antara lain, efisiensi konversi energi yang tinggi, mengurangi pemakaian bahan bakar minyak sehingga secara langsung dan mengurangi emisi gas buang ke atmosfir. Riset grup matertial maju dan energy storage fokus mengembangkan penelitian tentang produksi baterai dan aplikasinya. Kegiatan pengabdian ini bertujuan untuk mensosialisasikan hasil riset tentang baterai dan aplikasi kendaraan listrik sebagai salah satu cara transfer pengetahuan teknologi untuk pelajar Sekolah Menengah Kejuruan (SMK). Siswa SMK harus dibekali dengan pemahaman mengenai baterai lithium ion dan kendaraan listrik sehingga bisa meningkatkan kompetensi lulusan dan memiliki daya saing di pasar kerja. SMK Muhammadiyah 6 Karanganyar memiliki jurusan Teknik Audio Video, Teknik Komputer Jaringan, Teknik Mesin, Teknik Elektro dan Mekanik Otomotif sehingga kegiatan dan kerjasama ini akan sangat mendukung kegiatan pembelajarn. Kegiatan pengabdian ini merupakan tindak lanjut kerja sama magang siswa yang dilakukan di unit produksi baterai dibawah Pusat Unggulan Iptek (PUI) PT Teknologi Penyimpanan Energi Listrik (University Center of Excellence for Electrical Energy Storage Technology). Dengan terselenggaranya kegiatan pengabdian diharapkan mampu memberikan pengetahuan mengenai hasil riset kampus kepada siswa, sehingga dapat memberikan pemahaman mengenai konsep dasar kendaraan listrik dan menumbuhkan inovasi pada siswa untuk mengembangkan kendaraan listrik. Abstract. Electric vehicles are vehicles that are driven by electric motors from the battery as energy sources. The advantages of electric vehicles related to their high energy conversion include reducing fuel oil consumption and reducing exhaust emissions. The advanced materials and energy storage research group is currently developing researches on battery production and its applications. This educational activity is a part of the Research Group Service Grant (HGR-UNS) which aims to disseminate the results of research on batteries and their application to electric vehicles as a form of advanced technology transfer for Vocational High School (SMK) students. SMK students must be provided with knowledge about lithium-ion batteries (LIB) and electric vehicles so that they can improve their competence and increase their competitiveness in the job market. SMK Muhammadiyah 6 Karanganyar offers several programs so that this educational activity will greatly support students' learning activities. This education activity is also the continuation of interns' activities at the Center for Excellence in Higher Education Science and Technology for Electrical Energy Storage Technology. With this educational activity's implementation, we wish to increase students' knowledge about battery technology and its applications. Keywords: education; Lithium-Ion Battery; Electric Vehicle

Synthesis and Characterization of Material LiNi0.8Co0.15Al0.05O2 Using One-Step Co-Precipitation Method for Li-Ion Batteries Cornelius Satria Yudha; Luthfi Mufidatul Hasanah; Soraya Ulfa Muzayanha; Hendri Widiyandari; Agus Purwanto
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 4, No 3 (2019): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Li-ion battery is an energy storage device which could be applied as power source for electronic devices. The capacity of a battery is determined by the cathode material. Over this last decade, high nickel content cathode material is applied for electric vehicular technology. This study aims to synthesize a nickel-rich cathode material, LiNi0.8Co0.15Al0.05O2 (NCA) via one-step co-precipitation and study its characteristics. The Ni, Co and Al metal ion conversion during co-precipitation were analyzed using Atomic Adsorption Spectroscopy (AAS). Based on X-Ray diffraction analysis, NCA sample exhibited hexagonal-layered structure with high crystallinity. Based on Scherrer equation, the mean crystallite diameter of NCA sample is 40 nm. Scanning electron microscope (SEM) showed micron-sized homogenous particles with smooth surface. The final composition of Ni, Co and Al metal were confirmed using XRF. The capacity of the battery was determined using galvanostic test method with voltage range of 2.7-4.25 V using graphite as the counter anode. The initial specific discharge capacity of NCA is 60 mAh/g while the capacity loss per cycle is 1%.

Effect of Heating on the Pretreatment Process for Recycling Li-Ion Battery Cathode Soraya Ulfa Muzayanha; Cornelius Satria Yudha; Luthfi Mufidatul Hasanah; Adrian Nur; Agus Purwanto
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 4, No 2 (2019): JKPK ( Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

The use of Li-ion batteries has increased with the increasing of portable electronic media. Li-ion batteries have a life cycle hence a recycling process is needed in order to reduce the potential hazard of waste while increasing the economic value of unused battery material, especially its cathode active material. This study used Lithium Nickel Cobalt Oxide (NCA) cathode scrap to be regenerated which NCA material has high energy density and high capacity. The pretreatment process is one of the determinants in the subsequent recycling process. In this study, the effect of heating on the pretreatment process was carried out with variation temperatures of 500-8000C to obtain powder which will be recycled. The combination process of the leaching and co-precipitation was used to regenerate the cathode active material. Atomic Absorption Spectrophotometry (AAS) was performed to determine leaching efficiency using 4M H2SO4 at 400C for 3 hours. X-ray Diffraction (XRD) analysis showed that NCA material has been successfully regenerated which the diffraction peaks of NCA material was in accordance with JCPDS standards. The morphology of NCA material was tested using Scanning Electron Microscopy (SEM). Electrochemical testing uses a cylindrical battery at 2.7-4.2 Volt which the initial specific discharge capacity of the power is 62.13 mAh / g.

Influence Comparison of Precursors on LiFePO4/C Cathode Structure for Lithium Ion Batteries Luthfi Mufidatul Hasanah; Cornelius Satria Yudha; Soraya Ulfa Muzayanha; Diajeng Putri Suciutami; Atika Aulia Novita Sari; Inayati Inayati; Agus Purwanto
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 5, No 1 (2020): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Electricity is the most energy demanded in this era. Energy storage devices must be able to store long-term and portable. A lithium ion battery is a type of battery that has been occupied in a secondary battery market. Lithium iron phosphate / LiFePO4 is a type of cathode material in ion lithium batteries that is very well known for its environmental friendliness and low prices. LiFePO4/C powder can be obtained from the solid state method. In this study the variables used were the types of precursors : iron sulfate (FeSO4), iron oxalate (FeC2O4) and FeSO4+charcoal. Synthesis of LiFePO4/C powder using Li:Fe:P at 1:1:1 %mol. Based on the XRD results, LiFePO4/C from FeSO4+charcoal shows the LiFePO4/C peaks according to the JCPDS Card with slight impurities when compared to other precursors. XRD results of LiFePO4/C with precursors of FeSO4 or FeC2O4 shows more impurities peaks. This LiFePO4/C cathode is paired with lithium metal anode, activated by a separator, LiPF6 as electrolyte. Then this arrangement is assembled become a coin cell battery. Based on the electrochemical results, Initial discharge capacity of LiFePO4/C from the FeSO4 precursor is 19.72 mAh/g, while LiFePO4/C with the FeC2O4 precursor can obtain initial discharge capacity of 17.99 mAh/g, and LiFePO4/C with FeSO4+charcoal exhibit initial discharge capacity of 21.36 mAh/g. This means that the presence of charcoal helps glucose and nitrogen gas as reducing agents.

Utilization of Spent Nickel Catalyst as Raw Material for Ni-Rich Cathode Material Shofirul Sholikhatun Nisa; Anisa Raditya Nurohmah; Cornelius Satria Yudha; Hanida Nilasary; Hartoto Nursukatmo; Endah Retno Dyartanti; Agus Purwanto
Jurnal Presipitasi : Media Komunikasi dan Pengembangan Teknik Lingkungan Vol 18, No 2 (2021): July 2021
Publisher : Universitas Diponegoro

Spent nickel catalyst will be harmful to the environment if it is not processed or used properly. In fact, this waste still has a high nickel content. The treatment of spent nickel catalysts has been widely reported, but limited to nickel extraction. Since the lithium-ion batteries demand is continued to increase, then nickel is the most sought-after metal. Consequently, nickel from spent nickel catalysts could be developed as secondary source for lithium-ion battery cathode. This study aims to utilize spent nickel catalysts into more valuable materials. Nickel that has been extracted and mixed with Mn and Co has been used as raw material for nickel-rich cathode, namely NMC. Nickel extraction and NMC synthesis were using the acid leaching method followed by co-precipitation[WI1] [SSN2] . Based on the functional test performed in this work, nickel from spent nickel catalyst can be applied to Li-ion batteries. The sintering temperature that gives good characteristics and electrochemistry was found 820oC. The galvanostatic charge-discharge test gave specific capacity results for NMC of 110.4 mAh/g. The cycle test showed that NMC synthesized from spent nickel catalyst can be carried out up to 50 cycles with a capacity retention of 87.18%.

Co-Authors Adrian Nur Adrian Nur Anatta Wahyu Budiman Anatta Wahyu Budiman Anisa Raditya Nurohmah Arif Jumari Arif Jumari Atika Aulia Novita Sari Cornelius Satria Yudha Cornelius Satria Yudha Diajeng Putri Suciutami Endah Retno Dyartanti Endah Retno Dyartanti Endah Retno Dyartanti Fitria Rahmawati Hanida Nilasary Hartoto Nursukatmo Hendri Widiyandari Inayati Inayati Inayati Inayati Larasati Larasati Luthfi Mufidatul Hasanah Luthfi Mufidatul Hasanah Luthfi Mufidatul Hasanah Shofirul Sholikhatun Nisa Soraya Ulfa Muzayanha Soraya Ulfa Muzayanha Soraya Ulfa Muzayanha Tika Paramitha Tika Paramitha Witri Wahyu Lestari Wulan Cahya Inayah

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