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Ahmad Maulidi
Teknik Kimia, Institut Teknologi Kalimantan, Balikpapan
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology

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Journal : Agrointek

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Optimasi proses degumming minyak sawit mentah (DRPO) dengan response surface methodology (RSM) berbasis central composte design (CCD) Jefri Pandu Hidayat; Rizka Lestari; Siti Munfarida; Andini Angelina Putri; Adrian Prananda Putra; Fidela Chosta; Ahmad Maulidi
AGROINTEK Vol 19, No 2 (2025)
Publisher : Agroindustrial Technology, University of Trunojoyo Madura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21107/agrointek.v19i2.26063

Abstract

Crude palm oil (CPO) is widely used in various processed food products, especially cooking oil. Refining cooking oil involves high heating temperatures and the addition of bleaching earth, which aims to remove the sap and brown-red color. As a result, it can eliminate the carotene, which is not functionally used for good human metabolism. This research aims to remove sap and impurities in CPO by analyzing the optimal operation of heating temperature (60-80 °C) and phosphoric acid concentration (0.5-2 ml) and comparing the functional group change on the degumming process. The analytical method used was Response Surface Technology (RSM) by Central Composite Design (CCD) at Design Expert 12, which used carotene, density, and free fatty acid (FFA) responses. The results are optimal variables on heating temperature 80 °C and 2 ml of phosphoric acid concentration. The result of %FFA in DRPO was 1.917 %, the carotene was 381,350 ppm, and the density was 0.909 g/l. Heating temperature influences the FFA content, which is an important consideration. Higher temperatures can lead to an increase in FFA content. Indeed, lipase activation significantly affects the FFA content by accelerating the enzyme-catalyzed reaction. Apart from that, the addition of phosphoric acid affects the increase in FFA due to the non-reaction of phosphoric acid. The physicochemical characteristics of palm oil after the degumming process have not changed significantly, with the density before and after the degumming process still being in the range of (0.909–0.912) g/l. Group bonds have no change because the C-H and C=O group bonds in the main triglyceride compound. It requires a lot of energy to break the triglyceride cluster chains. The preliminary FFA model was revealed y=0.169\left(T\right)-0.1064\left(V\right)-1.5 to degummed reactor design, further.
Optimasi proses degumming minyak sawit mentah (DRPO) dengan response surface methodology (RSM) berbasis central composte design (CCD) Jefri Pandu Hidayat; Rizka Lestari; Siti Munfarida; Andini Angelina Putri; Adrian Prananda Putra; Fidela Chosta; Ahmad Maulidi
AGROINTEK Vol 19, No 2 (2025)
Publisher : Agroindustrial Technology, University of Trunojoyo Madura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21107/agrointek.v19i2.26063

Abstract

Crude palm oil (CPO) is widely used in various processed food products, especially cooking oil. Refining cooking oil involves high heating temperatures and the addition of bleaching earth, which aims to remove the sap and brown-red color. As a result, it can eliminate the carotene, which is not functionally used for good human metabolism. This research aims to remove sap and impurities in CPO by analyzing the optimal operation of heating temperature (60-80 °C) and phosphoric acid concentration (0.5-2 ml) and comparing the functional group change on the degumming process. The analytical method used was Response Surface Technology (RSM) by Central Composite Design (CCD) at Design Expert 12, which used carotene, density, and free fatty acid (FFA) responses. The results are optimal variables on heating temperature 80 °C and 2 ml of phosphoric acid concentration. The result of %FFA in DRPO was 1.917 %, the carotene was 381,350 ppm, and the density was 0.909 g/l. Heating temperature influences the FFA content, which is an important consideration. Higher temperatures can lead to an increase in FFA content. Indeed, lipase activation significantly affects the FFA content by accelerating the enzyme-catalyzed reaction. Apart from that, the addition of phosphoric acid affects the increase in FFA due to the non-reaction of phosphoric acid. The physicochemical characteristics of palm oil after the degumming process have not changed significantly, with the density before and after the degumming process still being in the range of (0.909–0.912) g/l. Group bonds have no change because the C-H and C=O group bonds in the main triglyceride compound. It requires a lot of energy to break the triglyceride cluster chains. The preliminary FFA model was revealed y=0.169\left(T\right)-0.1064\left(V\right)-1.5 to degummed reactor design, further.
Penentuan kondisi optimal operasi deodorisasi bertahap untuk memaksimalkan retensi karoten dalam produksi minyak sawit merah (RPO) Jefri Pandu Hidayat; Siti Munfarida; Rizka Lestari; Asful Hariyadi; Adrian Prananda Putra; Andini Angelina Putri; Ahmad Maulidi
AGROINTEK Vol 20, No 1 (2026)
Publisher : Agroindustrial Technology, University of Trunojoyo Madura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21107/agrointek.v20i1.25867

Abstract

Red palm oil (RPO) is an intermediate superfood derived from palm oil, with the potential to reduce stunting and supply sustainable phytonutrients aligned with SDGs 4 in Ibu Kota Nusantara (IKN), East Kalimantan. RPO contains significantly higher carotene levels than commercial oils which is produced through physical modification processes to remove phospholipids and palm distinctive smell by beta-ionone. This study focuses on optimizing the deodorization process that removing impurity and volatile compounds. The optimization used Response Surface Methodology (RSM) with Central Composite Design (CCD) across 13 experimental runs, varying two key parameter temperature (118–133°C) and heating time (238–253 minutes). The novelty of deodorization process using multi-flash autovaporization by lower temperature for better preserve carotene. The effects on carotene content, free fatty acids (FFA), and density were analyzed using Design Expert 13 software. The optimal condition was found at 120°C for 240 minutes, resulting in 280 ppm carotene, 1.11% FFA, and a density of 0.948 g/cm³. The carotene kinetic model has been foundwhere X is temperature and Y is time. Statistical and graphical analysis confirmed that the final product met Indonesian standards SNI 3741:2013 and 9098:2022, which require FFA below 5% and carotene above 30 ppm.
Co-Authors Adrian Prananda Putra Andini Angelina Putri Asful Hariyadi Fidela Chosta Jefri Pandu Hidayat Rizka Lestari Rizka Lestari Rizka Lestari Siti Munfarida Siti Munfarida