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SINTESIS SELULOSA DARI LIMBAH AMPAS TEBU (Saccharum Officinarum L.) DENGAN METODE HIDROLISIS ASAM DAN ULTRASONIKASI Balqis Saniatul Mukarromah; Maharani, Dina Kartika
Unesa Journal of Chemistry Vol. 14 No. 1 (2025): Vol 14 No 1 (2025)
Publisher : Department of Chemistry, Faculty of Mathematics and Natural Sciences, Surabaya State University, located at Jl Ketintang, Surabaya, East Java, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26740/ujc.v14n1.p28-32

Abstract

The annual increase in sugar factory production can lead to a yearly rise in bagasse waste. An alternative to minimize the increase in bagasse waste is to utilize it as nanocellulose. Bagasse contains 52.7% cellulose, 20% hemicellulose, and 24.2% lignin. The synthesis of nanocellulose was carried out using a combination of chemical and mechanical methods, namely acid hydrolysis and ultrasonication, resulting in a final yield of 39.96%. The FTIR spectra of raw bagasse and bagasse-derived nanocellulose showed changes indicating that the synthesis successfully removed non-cellulosic components such as lignin and hemicellulose. After the nanocellulose synthesis process, a small shoulder appeared at a 2θ angle of 14.5˚, indicating that the synthesis had successfully removed most of the amorphous structures such as lignin and hemicellulose. The nanocellulose from bagasse exhibited two diffraction peaks at 2θ angles of 16.2˚ and 22.2˚, which are characteristic of type I cellulose.