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All Journal African Multidisciplinary Journal of Sciences and Artificial Intelligence
Eneji I. S
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Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Environmental Science Materials Science & Nanotechnology

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Green Synthesis, Structural Characterization and Study of Thermal Behaviour of Cu2+ and Co2+ Complexes Derived from Salicylidene-3-Amino Benzoic Acid Ama S. O; Wuana R. A; Sha’ato R; Eneji I. S
African Multidisciplinary Journal of Sciences and Artificial Intelligence Vol 1 No 1 (2024): African Multidisciplinary Journal of Sciences and Artificial Intelligence
Publisher : Darul Yasin Al Sys

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.58578/amjsai.v1i1.3741

Abstract

The Schiff base ligand Salicylidene-3-amino benzoic acid (SAB) was prepared by reacting salicylaldehyde with 3-amino benzoic acid. Its Cu2+ and Co2+ complexes were prepared by reacting ethanolic solutions of SAB with magnetically stirred solution of metal salts in distilled water using microwave-assisted heating for 30 min. The ligand and complexes were characterized on the basis of physical properties, FT-IR, UV-Vis, magnetic susceptibility, XRD and TGA/DTA. Unit cell dimensions obtained from XRD crystallography analysis agreed with the establishment of orthorhombic crystal structure. The spectroscopic studies revealed the presence of -C=N, -C=O, M-O, M-N, -OH and NO3 functional groups and this showed that the ligand coordinated to metal via N and O donors. The thermal decomposition of the complexes indicates the loss of lattice of water and decomposition of the ligand as key to the interpretation of successive weight loss.
Co-Authors Ama S. O Sha’ato R Wuana R. A