Jurnal Kimia (Journal of Chemistry)
Vol. 7, No. 2 Juli 2013

STUDI REAKSI SIKLOPENTILSILAN DENGAN 4-IODIDA THIOANISOL MENGGUNAKAN KATALIS PALADIUM

Aldes Lesbani (Unknown)
Risfidian Mohadi (Unknown)
Elfita Elfita (Unknown)

Article Info

Publish Date
01 Jul 2013

Abstract

A study on cyclopentylsilane reaction in tetrahydrofuran with 4-iodo thioanisol has been carried out using palladium as catalyst under argon atmosphere at room temperature. The results showed that the product was tris(4-thioanisyl)cyclopentylsilane (1) which was obtained from recrystallization using methanol with the yield 35%. The Compound (1) has a melting point of 91.5-92.0 oC. Analysis using GC-MS found m/z 466 with six equivalent protons and eight carbons peak obtained from 1H and 13C NMR.

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Journal Info
Jurnal Kimia (Journal of Chemistry)
Website

Abbrev

jchem

Publisher

Universitas Udayana

Subject

Chemistry

Description

Jurnal Kimia (Journal of Chemistry) publishes papers on all aspects of fundamental and applied chemistry. The journal is naturally broad in scope, welcomes submissions from across a range of disciplines, and reports both theoretical and experimental ...