Jurnal Kimia (Journal of Chemistry)
Vol. 5, No. 2 Juli 2011

QUALITY CONTROL OF GC PERFORMANCE FOR STEROID ANALYSIS

Iryanti Eka Suprihatin (Unknown)



Article Info

Publish Date
14 Nov 2012

Abstract

This paper reports the process conducted to maintain a high quality of GC responses in obtaining reliabledata on steroid analyses of environmental samples. Works including setting up the Limit of Detection (LOD) andLimit of Quantitation (LOQ), maintaining linearity, controlling the reproducibility, and determining its reliability aredescribed. It is evident that in this work the LOD of the GC is 0.0002 ng (by 1 mL injection of 0.2 mgL-1 samples) andthe LOQ is 0.001 ng (by 1 mL injection of 1 mgL-1 samples), which means it is capable of detecting much lowerconcentrations of steroid compounds if the samples undergo 2000 times pre-concentration during preparation. Underthe range investigated the GC provides reliable quantitative linear responses to all steroid compounds.

Copyrights © 2011






Journal Info

Abbrev

jchem

Publisher

Subject

Chemistry

Description

Jurnal Kimia (Journal of Chemistry) publishes papers on all aspects of fundamental and applied chemistry. The journal is naturally broad in scope, welcomes submissions from across a range of disciplines, and reports both theoretical and experimental ...