Jurnal Ilmu Dasar
Vol 8 No 1 (2007)

Adsorption of Pb (II) by Chitosan Resulted from Bakau Crab’s Shell (Scylla sp) Chitin Isolation

Indah Sanjaya (Jurusan Kimia FMIPA Universitas Negeri Surabaya)
Leny Yuanita (Jurusan Kimia FMIPA Universitas Negeri Surabaya)



Article Info

Publish Date
30 May 2013

Abstract

The aim of this research was to find the effect of interaction time on adsorption of Pb (II) by chitosan.The research was done in three stages: (i), the isolation of chitin from Bakau Crab’s Shell (Scylla sp); (ii), chitin deacetilation becomes chitosan; (iii), interaction of chitosan to Pb (II). Qualitative analysis was done by ninhidrin test, while quantitatively was carried out by infra red spectra. Langmuir Hinshelwood kinetica equation was applied to determine adsorption velocity of chitosan to Pb (II), and one way analysis of variance to determine the effect of interaction time to adsorption of Pb (II) (α = 5%). Interaction time was 10, 30, 50, 70, 90, 110, and 130 minutes. The results showed that: (a) deacetilation degree of chitin and chitosan were 35.94 and 65.28 % respectively, (b) ninhidrin test was resulting purple colour for chitosan, (c) period time of equilibrium to adsorp Pb (II) was 70 minutes. From Langmuir- Hinshelwood kinetica equation resulting that k1 = 0.0014 minutes-1 and K = 1189.6 M-1. Range of chitosan adsorption velocity to Pb (II) was 2977. 10-7 to 3.275. 10-7 mol/L minutes.

Copyrights © 2007






Journal Info

Abbrev

JID

Publisher

Subject

Control & Systems Engineering Mathematics

Description

Jurnal ILMU DASAR (JID) is a national peer-reviewed and open access journal that publishes research papers encompasses all aspects of natural sciences including Mathematics, Physics, Chemistry and Biology. JID publishes 2 issues in 1 volume per year. First published, volume 1 issue 1, in January ...