Indonesian Journal of Science and Technology
Vol 5, No 3 (2020): IJOST: VOLUME 5, ISSUE 3, 2020

Synthesis and Application of a Sulfonated Carbon Catalyst for a Hydrolisis Reaction

Efiyanti, Lisna (Unknown)
Indrawan, Dian Anggraini (Unknown)
Arif, Zulhan (Unknown)
Hutapea, Devandri (Unknown)
Septina, Ane Dwi (Unknown)



Article Info

Publish Date
01 Dec 2020

Abstract

Biomass, such as wood waste, is one of the resources that can be potentially converted into a carbon product for catalyst applications. In this study, the sulfonated carbon was obtained through the pyrolysis method for wood waste at the temperature of 350°C, which was later sulfonated through the use of  H2SO4 (8N) on the reflux for 4 h. The sulfonated carbon was then analyzed and characterized including its water content, ash content, volatile matter, fixed carbon, iodine adsorption as well as the H+ (acidity) capacity using ammonia adsorptions and functional groups and the Fourier Transform Infra-Red (FTIR) instrument. The catalyst application was carried out during the kempili pulp hydrolysis process using a microwave with the ratio of catalyst to a pulp of 1:1 (5g:5g), with the power conditions of 300, 400, and 600 watt for 3, 5, and 7 min. The results showed that the sulfonated carbon catalyst had water content, volatile matter, ash content, fixed carbon, iodine adsorption as well as the catalyst acidity as much as 3.48%; 11.70%; 4.21%; 84.62%; 690.88 mg/g; and 6.45 mmol/g, respectively with the highest glucose content of 160.83 ppm. The carbon-based catalyst is expected as an alternative catalyst, can be further developed for hydrolysis reactions, and can serve as a green technology product in the future.

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