Chemistry Indonesian Journal of Chemical Research
Vol 3 No 1 (2015): Edisi Bulan Juli (Edition For July)

Preparation and Characterization Ni-Mo/Montmorillonite As A Catalyst In Cracking Process

Sopiarini, Putri (Unknown)
Firdaus, Firdaus (Unknown)
Taba, Paulina (Unknown)



Article Info

Publish Date
31 Jul 2015

Abstract

This research is aims to prepare and characterization of montmorillonite intercalated Ni-Mo as a catalyst in the cracking process. Preparation is do by extracting monmorillonite of bentonite by decantation method. Monmorillonite synthesized with NaCl to obtain Na-monmorillonite. Ni-Mo/monmorillonite obtained by dissolving ammonium hepta molybdate (NH4)6Mo7O24.4H2O) with distilled water and refluxed with Na-monmorillonite for 6 hours and dried at a temperature of 120oC. Furthermore, nickel nitrate hexahydrate (Ni(NO3)2.6H2O) is dissolved in distilled water and refluxed with Mo-monmorillonite for 6 hours and dried at a temperature of 120oC. Ni-Mo/monmorillonite obtained is then calcined at a temperature of 600oC for 4 hours to activate and eliminate the remnants of organic materials. Characterization of Ni-Mo/monmorillonite do by XRD, XRF and SEM. Characterization by XRD showing the change in the content of monmorillonite, Na-monmorillonite, and Ni-Mo/monmorillonite. Characterization by XRF confirms the success of the creators do with increasing metal content of Ni and Mo in monmorillonite replace the position of the metal Na. Characterization by SEM showed highly significant differences in morphology of montmorillonite, Na-monmorillonite and Ni-Mo-monmorillonite

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Journal Info

Abbrev

Indonesian Journal of Chemical Research (Indones.

Publisher

Subject

Biochemistry, Genetics & Molecular Biology Chemistry Engineering Environmental Science

Description

Indo. J. Chem. Res. is a journal that regularly publishes primary articles covering all branches of chemistry and its sub-disciplines. Published articles consist of complete research, short communication, and review articles. The scope of published articles is not limited to inorganic chemistry, ...