Sintesis dan Karakterisasi Fe₂TiO₅ dari Besi Oksida dan Titanium Dioksida dengan Metode Planetary Ball-Mill: Synthesis and Characterization of Fe₂TiO₅ from Iron Oxide and Titanium Dioxide Using the Planetary Ball-Mill Method

Laode Kadir
M. H Azis (Jurusan Kimia, Universitas Mataram)
S. Musiam (Jurusan Kimia, Sekolah Tinggi Ilmu Kesehatan ISFI Banjarmasin)
V. A. Fabiani (Jurusan Kimia, Universitas Bangka Belitung)
Karnelasatri (Jurusan Farmasi, Universitas Pelita Harapan)
D. Permana (Jurusan Kimia, Universitas Sembilan Belas November Kolaka)
T Azis (Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam,Universitas Halu Oleo)
Syahrir (Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam,Universitas Halu Oleo)

KOVALEN: Jurnal Riset Kimia
Vol. 8 No. 3 (2022): December Edition

The method of solid hydrogen storage through integration in metal hydride compounds is a new, promising method. This research has succeeded in synthesizing and characterizing the metal hydride alloy Fe-Ti system through a planetary ball-mill process. Based on the XRF analysis, it was found that the composition of Fe oxide content reached 56.22% while Ti oxide reached 43.78%. The FTIR study showed absorption at wavenumbers of 900 cm-1 and 500 cm-1. Both are typical absorptions for Ti-O and Fe-O groups, suggesting that the synthesized sample was successful. It can be seen from the XRD data that some of the diffractogram peaks of the resulting Fe-Ti compound match the peaks of the Fe2TiO5 and TiO2 compounds obtained from the Powder Diffraction File (PDF) database number 00-003-0374. After the refinement was performed, information was obtained that the synthesis of Fe-Ti alloy material using the planetary ball mill technique produced Fe2TiO5.