JURNAL PENELITIAN SAINTIKA
VOL 15, NO 2 (2014): JURNAL PENELITIAN SAINTIKA

PREPARASI BENTONIT ALAM MENJADI NANO PARTIKEL

Bukit, Nurdin (Unknown)
Ginting, Eva Marlina (Unknown)
Harahap, Mukti Hamjah (Unknown)



Article Info

Publish Date
07 Apr 2016

Abstract

The purpose of this study is the manufacture of natural bentonite into  nano  particles  and  is  used  as  a  filer  on  thermoplastic  high-density polyethylene  (  HDPE  )  .  The  method  used  in  the  manufacture  of  nanoparticles  of  bentonite  are  two  ways  ;  The  first  synthesis  method  using surfactant  cetyl  trimethyl  ammonium  bromide  (  CTAB  )  and  the  second way  in  ballmill  for  10  hours  .  Characterization  of  the  particle  size analyzer  (  PSA  )  ,  morphological  analysis  with  scanning  electron microscope ( SEM ) and analysis of the structure by X  -  ray diffraction ( XRD  )  was  performed  .  Nano  particles  with  variation  of composition  of natural  bentonite  (  2  ,  4  ,  6  ,  8  ,  10  %  w  t)  blends   with  HDPE  and compatibilizer  PE  -  g-  MA  on  the  appliance  s  internal  mixer  at  a temperature  of  150oC  and  laboplatomil  rate  of  60  rpm  for  10 minute.Berdasarkan PSA analysis and X  -  ray , natural bentonite having an average size of 75 nm for synthesis with CTAB , and 97.5 nm for the ball  mill  .  from  the  results  of  XRD  analysis  of  minerals  crystoballite  ( SiO2 ) and phase annite ( Al3.448Fe3K0.99Na  0.01O12Si  2.552  ) . In testing the mechanical  properties  of  the  resulting  increase  in  tensile  strength  and breaking up the composition perpajangan 2 to 6 % and a decline in the composition  of  8  %  .  The  results  of  SEM  analysis  showed  that homogeneous  mixing  of  ingredients  and  the  bentonite  particle agglomeration on the composition of 10 % wt.

Copyrights © 2014