Jurnal Teknik
Vol 23 No 1 (2024): Jurnal Teknik - Media Pengembangan Ilmu dan Aplikasi Teknik

Model Efisiensi Arus pada Elektrolisis Serbuk Tembaga Menggunakan Metode Perancangan Percobaan Faktorial Desain 2K

Gunawan, R. Mohamad Fajar (Unknown)
Soleh Wahyudi (Unknown)
Andrie Harmaji (Unknown)
Diana Kamaliyah Ichsan (Unknown)
Gigih Safardwiyansyah (Unknown)
Naufal Dhiya Ulhaq (Unknown)



Article Info

Publish Date
19 Jun 2024

Abstract

This paper presents the results of developing a current efficiency model for copper powder electrolysis and analyzes the factors that most influence current efficiency using a 2K factorial experimental design. The three independent variables are copper ion (Cu) concentration, current density, and electrolysis time. Copper powder electrolysis experiments were conducted using a pure copper plate anode (99.88% Cu) and a 316L stainless steel cathode. Current efficiency is calculated based on data on the weight of the copper powder produced. Copper powder characterization uses a Scanning Electron Microscope (SEM) to determine the morphology and size distribution of the powder, X-ray Diffraction (XRD) to identify powder phases/compounds, Energy Dispersive X-ray Spectroscopy (EDX) to analyze the elemental composition and Particle Size Analyzer ( PSA) to determine the powder particle size and distribution. The prediction model obtains the highest current efficiency at 96%. The resulting copper powder has a dendritic structure morphology with an average particle size of 114.9 µm. It comprises cuprite (Cu2O) and copper (Cu) with a composition of 88.17% Cu and 11.83% O.

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