Jurnal Bahan Alam Terbarukan
Vol 6, No 1 (2017): June 2017 [Nationally Accredited]

SYNTHESIS OF SILVER NANOPARTICLES FROM SILVER NITRATE SOLUTION USING GREEN TEA EXTRACT (CAMELIA SINENSIS) AS BIOREDUCTOR

Rengga, Wara Dyah Pita ( Chemical Engineering Department, Fakultas Teknik, Universitas Negeri Semarang, Kampus Sekaran Gunung Pati, Semarang 50229, Indonesia)
Yufitasari, Arie ( Chemical Engineering Department, Fakultas Teknik, Universitas Negeri Semarang, Kampus Sekaran Gunung Pati, Semarang 50229, Indonesia)
Adi, Wismoyo ( Chemical Engineering Department, Fakultas Teknik, Universitas Negeri Semarang, Kampus Sekaran Gunung Pati, Semarang 50229, Indonesia)



Article Info

Publish Date
02 Jun 2017

Abstract

The synthesis of silver nanoparticles with micro size is highly required in antibacterial fields. The biorefinery material is highly potential as a bioreductor which is applied in the synthesis of nanoparticles. The bioreductor is made from green tea leaves extraction using aquadest to extract its active substance, the catechin which is derived from polyphenol. The polyphenol can reduce the synthesis of silver nanoparticles naturally. The result of FTIR analysis from green tea leaves extract containing polyphenol shown in the uptake functional groups is -OH group located in 3425 cm-1, C=O group located in 1635 cm-1, C=C group located in 1527, and 1442 cm-1 , and C-O group located in 1234 cm-1. The precursors of AgNO3 was used as the main synthetic material. The synthetic condition was resulted from the reaction between the extraction of green tea extract and AgNO3 as the precursors in the variation of synthetizing time. The heating process during synthesizing is done in 50 ˚C along with stirring to foster the creation of silver nanoparticles. The analysis result of XRD shows that silver nanoparticles has the diffraction peaks in the angle of 2 theta that are 44.08, 64.40, and 77.51. The types of silver nanoparticles is Ag0 nanoparticles with face-centered cubic crystal structure. Based on TEM analysis, the size and particle size distribution can be determined using image J. The distribution shows that the longer synthesizing time, the bigger nanoparticles produced. With synthesizing times at 24 hours, 6 hours, 3 hours, and 2 hours produce average particle size of 26.4 nm; 9.2 nm; 8.4 nm; and 7.4 nm respectively.

Copyrights © 2017






Journal Info

Abbrev

jbat

Publisher

Subject

Materials Science & Nanotechnology

Description

This journal presents articles and information on research, development and applications in biomass conversion processes (thermo-chemical conversion; physico-chemical conversion and bio-chemical conversion) and equipment to produce fuels, power, heat, and value-added chemicals from biomass. A ...