This study aims to synthesize and characterize composites based on Pahae Natural Zeolite and Durian Peel Activated Carbon as phosphate reducers in laundry wastewater. Zeolite was activated using 1 M NaCl solution, while activated carbon was prepared by carbonization at 500 °C for 2 hours. The Zeolite–Activated Carbon mixtures were prepared with compositions of 100%:0%, 95%:5%, 90%:10%, 85%:15%, 80%:20%, 75%:25%, and 0%:100%, pressed at 6 tons for 10 minutes, and sintered at 700 °C, 800 °C, and 900 °C for 4 hours. Characterization included physical properties (porosity, water absorption), mechanical properties (hardness), morphology (SEM), crystal structure (XRD), and elemental composition (XRF). The results showed that the optimum condition was achieved at a 75%:25% composition and 700 °C, with porosity of 59.67%, water absorption of 56.06%, and phosphate reduction efficiency of 80.86%. The highest hardness value was obtained at 100%:0% composition at 900 °C, reaching 784.14 MPa. Therefore, the Pahae Natural Zeolite–Durian Peel Activated Carbon composite demonstrates potential as an effective and environmentally friendly adsorbent for wastewater treatment.
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