Journal Serambi Engineering (JSE)
Vol. 11 No. 2 (2026): April 2026

Synthesis and Characterization of Silica from Lapindo Mud Waste with Acid and Base Solvents

Riesnawa, Yurdien Dellan (Unknown)
Azaria, Atha Nur (Unknown)
Reva Edra Nugraha (Unknown)



Article Info

Publish Date
21 Mar 2026

Abstract

Lapindo mud is a geological waste product resulting from the mud eruption in Sidoarjo, East Java, Indonesia, which continues to raise environmental concerns. However, this material has considerable potential due to its high silica (SiO2) content. This study evaluates the effectiveness of acid leaching and alkaline precipitation methods for extracting silica from Lapindo mud and investigates the properties of the resulting silica. Acid leaching was conducted using HCl (4, 8, and 10 M), while alkaline treatment employed NaOH (2, 6, 8, 10, and 12 M) and KOH (8, 10, and 12 M). The results showed that acid leaching is effective in removing metallic impurities without dissolving the silica framework, resulting in only a limited increase in SiO2 content from 54% to 57%. On other hand, silica purity was greatly increased by precipitation using a base solvent; the maximum SiO2 content was achieved at 97.5% with 10M NaOH. Nitrogen adsorption-desorption analysis shows that the precipitated silica had mesoporous properties with a type IV isotherm and an average pore size of 20.60 nm, while XRD analysis verifies the conversion of crystalline silica into amorphous silica. Thus, the most efficient technique for generating high-quality silica from Lapindo mud waste is alkaline precipitation with 10M NaOH

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Journal Info

Abbrev

jse

Publisher

Subject

Earth & Planetary Sciences Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering

Description

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