The Journal of Pure and Applied Chemistry Research
Vol 6, No 3 (2017): Edition of September - December 2017

Synthesis and Characterization of Polyaniline Nanoparticle by Inverse Micelle Microemulsion Method

Nuraini Uswatun Chasana (Brawijaya University)
Siti Mariyah Ulfa (Brawijaya University)
Masruri MASRURI (Brawijaya University)



Article Info

Publish Date
01 Sep 2017

Abstract

Polyaniline (PANI) is a conductive polymer and potential for application in the electronic device manufacturing. This paper discloses a recent strategy in synthesis polyaniline nanoparticle (NP-PANI) using inverse micelle (IM) microemulsion method, and also characterization of the provided products. The synthesis step was conducted by mixing of aniline as a polymer precursor with PEG 400, n-hexane, n-butanol, ammonium persulfate and hydrochloric acid in three different reaction times, i.e. for 2, 6, and 12 hours at 26 oC. NP-PANI was afforded as a brown powder in 2.87%, 1.97% and 2.30% yield for NP-PANI-IM-2, NP-PANI-IM-6 and NP-PANI-IM-12. The characteristic on ultra violet-visible and infrared spectra exhibited NP-PANI was formed as an emeraldine salt oligomer. Moreover, their morphology was observed through scanning electron microscopy (SEM) and showed a different range of nanoparticle size, i.e. 50-62, 68-72 and 58-62 nm for NP-PANI-IM-2, NP-PANI-IM-6 and NP-PANI-IM-12, respectively. These products open the potency application in material science.

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Journal Info

Abbrev

jpacr

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology Medicine & Pharmacology

Description

The Journal of Pure and Applied Chemistry Research focuses in publishing research articles in the field of Chemistry and Applied Chemistry. The target is in exploring, investigating, and developing chemicals sources from local and/or Indonesian to increase the value. Scope of the journal is organic ...