Techno: Jurnal Penelitian
Vol 15 No 1 (2026): TECHNO JURNAL PENELITIAN

Performance Evaluation of the Karl Fischer Method for Determining Water Content in Food Products

Ardina Purnama Tirta (Politeknik AKA Bogor)
Imas Solihat (Politeknik AKA Bogor)
Regy Reynaldi (Politeknik AKA Bogor)
Achmad Nandang Roziafanto (Politeknik AKA Bogor-Ministry of Industry)



Article Info

Publish Date
31 May 2026

Abstract

Water content is a crucial parameter in determining the quality of food products, as it influences physicochemical properties, microbial growth, and shelf life. Therefore, reliable methods for water content determination are essential. This study evaluated the performance of the Karl Fischer method through several parameters: linearity, limit of detection (LOD), limit of quantitation (LOQ), precision, accuracy, and measurement uncertainty. The method showed strong linearity with the regression equation y = 0.9719x + 0.5062 and a correlation coefficient (r) of 0.9998 across 1.0–10.0% water concentration. The LOD and LOQ were found to be 0.10% and 0.13%, respectively. Precision (%RSD) at 5, 60, and 100% water concentrations yielded values of 0.88, 0.26, and 0.09%. Accuracy (% trueness) ranged from 92% to 105%, while the mean relative uncertainty was 6%. These results demonstrate that the Karl Fischer method offers acceptable performance and is suitable for accurate water content determination in food products.

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Journal Info

Abbrev

techno

Publisher

Subject

Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Civil Engineering, Building, Construction & Architecture

Description

TECHNO: Jurnal Penelitian diterbitkan oleh Lembaga Penelitian dan Pengabdian Masyarakat (LPPM) Universitas Khairun, dua kali terbit dalam setahun dengan jumlah artikel dalam sekali terbit sebanyak 8 ...