Jurnal Polimesin
Vol 24, No 3 (2026): June

Effect of alkali fusion temperature on the synthesis and characteristics of nanosilica from silica sand

Muhammad Sadat Hamzah (Universitas Tadulako)
Muchsin Muchsin (Universitas Tadulako)
Abdul Muis (Universitas Tadulako)
Dino Hasyim (Universitas Tadulako)
Iqrham Dwi Putra Annas (Universitas Tadulako)
Muhammad Syaiful Fadly (Universitas Tadulako)
Bakri Bakri (Universitas Tadulako)
Sri Chandrabakty (Universitas Tadulako)



Article Info

Publish Date
30 Jun 2026

Abstract

The increasing demand for nanosilica in industrial applications has encouraged the utilization of abundant natural silica sand as a sustainable raw material. This study investigates the effect of alkali fusion temperature on the synthesis and characteristics of nanosilica derived from silica sand from Central Sulawesi, Indonesia. A cost-effective, energy-efficient synthesis method is needed to transform raw sand into high-value nanoparticles with controlled morphology. The study employed the alkali fusion method, where silica sand was reacted with NaOH at temperatures ranging from 400°C to 700°C, followed by leaching and titration to pH 7-8 to produce nanosilica. Characterization results via XRF and XRD confirmed that the synthesized nanosilica maintains a high SiO2 concentration (up to 72.46%) and exhibits a coexistence of amorphous phases and crystalline quartz. Morphological analysis by TEM revealed that increasing the fusion temperature decreases particle size from 18.91 nm at 400°C to 14.00 nm at 700°C, indicating that higher thermal energy promotes structural decomposition. These findings suggest that the alkali fusion temperature is an important parameter for controlling nanosilica dimensions. Further evaluation, including yield and recovery analysis, is required to assess process efficiency and its potential for large-scale applications.

Copyrights © 2026






Journal Info

Abbrev

polimesin

Publisher

Subject

Automotive Engineering Control & Systems Engineering Engineering Materials Science & Nanotechnology Mechanical Engineering

Description

Polimesin mostly publishes studies in the core areas of mechanical engineering, such as energy conversion, machine and mechanism design, and manufacturing technology. As science and technology develop rapidly in combination with other disciplines such as electrical, Polimesin also adapts to new ...