Indonesian Journal of Chemistry
Vol 8, No 2 (2008)

PREPARATION OF CHITOSAN-GOLD NANOPARTICLES: PART 1 (OF 2). EFFECT OF REDUCING TECHNIQUE

Adlim Adlim (Jurusan Kimia FKIP Universitas Syiah Kuala Darussalam, Banda Aceh, 23111)
Mohamad Abu Bakar (School of Chemical Sciences, Universiti Sains Malaysia, 11800 Minden, Penang)



Article Info

Publish Date
17 Jun 2010

Abstract

Chitosan-stabilized gold nanoparticles were synthesized in aqueous formic acid, citric, or acetic acid with and without chitosan as the stabilizer. Refluxing in methanol, addition of hydrazine or sodium borohydride, photo-irradiation were employed as the reducing agents & reduction technique of gold ions. Dispersed particles of chitosan-stabilized gold were obtained in aqueous acetic acid-methanol solution.  The chitosan-stabilized gold colloids (chi-Au) were dispersed and the particle size were in range of 9-30 nm, some of which were crystalline with various shapes.  Chi-Au prepared with hydrazine as the reducing agent resulted in large and aggregated particles. The finest and dispersed chi-Au particles were obtained if NaBH4 was used as the reducing agent and the diameters could be controlled within 2.2-2.3 nm.

Copyrights © 2008






Journal Info

Abbrev

ijc

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry

Description

Indonesian Journal of Chemistry is an International, peer-reviewed, open access journal that publishes original research articles, review articles, as well as short communication in all areas of chemistry including applied chemistry. The journal is accredited by The Ministry of Research, Technology ...