JURNAL PENELITIAN SAINTIKA
Vol 14, No 2 (2014): SEPTEMBER 2014

PREPARASI BENTONIT ALAM MENJADI NANO PARTIKEL SEBAGAI FILLER PADA TERMOPLASTIK HDPE

Bukit, Nurdin (Unknown)
Ginting, Eva Marlina (Unknown)
Harahap, Mukti Hamzah (Unknown)



Article Info

Publish Date
31 Jan 2019

Abstract

The purpose of this study is the manufacture of natural bentoniteinto nano particles and is used as a filer on thermoplastic high-densitypolyethylene ( HDPE ) . The method used in the manufacture of nano-particles of bentonite are two ways ; The first synthesis method usingsurfactant cetyl trimethyl ammonium bromide ( CTAB ) and the secondway in ballmill for 10 hours . Characterization of the particle sizeanalyzer ( PSA ) , morphological analysis with scanning electronmicroscope ( SEM ) and analysis of the structure by X - ray diffraction (XRD ) was performed . Nano particles with variation of composition ofnatural bentonite ( 2 , 4 , 6 , 8 , 10 % w t) blends with HDPE andcompatibilizer PE - g- MA on the appliance 's internal mixer at atemperature of 150 C and laboplatomil rate of 60 rpm for 10 minute.Berdasarkan PSA analysis and X - ray , natural bentonite having an average size of 75 nm for synthesis with CTAB , and 97.5 nm for the ball mill . from the results of XRD analysis of minerals crystoballite (SiO2 ) and phase annite ( Al3.448Fe3K0.99Na 0.01O12Si 2.552 ) . In testing the mechanical properties of the resulting increase in tensile strength and breaking up the composition perpajangan 2 to 6 % and a decline in the composition of 8 % . The results of SEM analysis showed that homogeneous mixing of ingredients and the bentonite particle agglomeration on the composition of 10 % wt. 

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