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Jurnal Teknik Kimia USU

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Published by Universitas Sumatera Utara

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Articles 10 Documents

Search results for , issue "Vol 5, No 2 (2016)" : 10 Documents clear

EKSTRAKSI LIKOPEN DARI BUAH TOMAT (Lycopersicum Esculentum) MENGGUNAKAN PELARUT TUNGGAL DENGAN METODE KRISTALISASI ANTISOLVENT Sola Fide Gavra Tarigan, Deviana C.S. Sinaga, Zuhrina Masyithah
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

This research was aimed to study the effect of feed and solvent ratio (f/s), antisolvent variety and solvent variety to the extraction of lycopene from tomato (Lycopersicum esculentum)by using single solvent and antisolvent crystalization method. The solvent that used was hexane and ethyl acetate and also methanol and ethanol as the antisolvent. Tomatoes was milled and then extracted. Antisolvent then added to the extract which was obtained. The results show that the more feed and solvent ratio (f/s) the more lycopene obtained. At the ratio of 1:4,5 with hexane as the solvent obtained the highest lycopene yield were 2,7 mg/150 ml and 2,2 mg/150 ml. Whereas at the ratio of 1:4,5 with ethyl acetate as the solvent obtained the highest lycopene yield were 3,2 mg/150 ml dan 2,8 mg/150 ml. By using methanol as an antisolvent, much lycopene would be obtained. By using ethyl acetate as a solvent, much lycopene would be obtained.

KARAKTERISTIK BRIKET DARI SEKAM PADI DAN KETAMAN KAYU BERPEREKAT DAUN JAMBU METE Widya Gema Bestari, Mutiara Mendopa, Rosdanelli Hasibuan
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

Briquettes are biomass compaction technology as alternative energy sources with or without binder in different shape and size. The research is aimed to analyze the best carbonization process, compaction pressure and binder concentration for quality of briquettes. In this resarch, rice husk and wood shaving are used as raw materials carbonized at different process, named by carbonization process 1 and other carbonization process 2. Carbonization process 1 was done by carbonized each raw material and then mixed while carbonization process 2 was done by mixed raw materials then carbonized. Raw materials were blended with cashew nut leaves binder at concentration 10%, 12,5%, 15%, and 20% and then compacted at pressure 85 kg/cm2 and 105 kg/cm2. The best briquette was briquette that rice husk and wood shaving were carbonized by carbonization process 1 blended with 15% binder and compacted at 85 kg/cm2 and had calorific value 2045,8271 cal/g.

PENGARUH KONSENTRASI RAGI DAN WAKTU FERMENTASI PADA PEMBUATAN BIOETANOL DARI BIJI CEMPEDAK (Artocarpus champeden spreng) Irvan, Ayu Wandira Putri, Sri Ulina Surbakti, Bambang Trisakti
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

Needs fuel as a source of energy every day is increasing, while the energy reserves of petroleum (fossil) dwindling, therefore, to meet the needs of the fuel it is necessary to develop alternative fuels that are renewable and home environment (renewable ). Etonal Bioethanol is made from plants containing starch, sugar and other plant cellulose. Where in this study using jackfruit seeds that contain high enough carbohydrates as raw materials. This research aims to make bioethanol from cempedak seeds with various concentrations of yeast and fermentation time. The main process is hydrolysis; fermentation using yeast Saccharomyces Cereviciae; and purification by distillation and condensation. Variables used are changes in the concentration of yeast 3%, 6%, 9% and 2 days, 3 days, 4 days fermentation period. From the analysis of the research results obtained bioethanol yield per amount of raw materials is the best starting 12,5 ml/kg with a density of 0.962 g/ml and the calorific value sebasar 181.925 kcal/kg, which is the variation of the concentration of 9% and 3 days of fermentation period.

PEMBAKARAN PREMIKS UAP MINYAK KELAPA DALAM HELE-SHAW CELL Hadi Saroso
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

Coconut oil combustion characteristic is observed experimentally by evaporating oil in the boiler then mix it with air before being burned at various equivalence ratios in the Hele-shaw cell. The result shows that, coconut oil tends to break into glycerol and fatty acid due to hydrolysis reaction producing the flame propagation, where the fatty acid flame propagates first then glycerol flame. Micro-explosion occurs when moisture from fatty acid combustion is absorbed by glycerol, and higher heating due to higher flame speed produces more micro-explosion.

PENGARUH BAHAN PENGISI SILIKA DAN SERBUK TANDAN KOSONG SAWIT (STKS) TERMODIFIKASI TERHADAP KEKUATAN BENTUR DAN DAYA SERAP AIR KOMPOSIT HIBRID POLIESTER TIDAK JENUH Halimatuddahliana, Johan Evander Sirait, Fermadi Sirait
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

This research aims to determine the effect of palm oil empty fruit bunches (POEFB) powder and silica into the matrix of unsaturated polyester resin (UPR) and the influence of chemical modification OPEFB with using acetic acid 50% (v / v). In this study, (UPR) was mixed with silica and OPEFB to weight ratio (UPR: Silica: OPEFB) 80: 20: 0, 80: 15: 5, 80: 10: 10, 80: 5: 15, 80: 0: 20 by hand lay-up method. Analysis was done by impact test, and analysis of scanning electron microscopy (SEM). Results showed that impact strength at a ratio of 80: 5: 15 was higher than those without modification viz. 3622.5 J / m2. In this case the chemical modification has lowered OPEFB polarity so that the interfacial tencion between the filler with a matrix became low resulting in good interfacial interaction and adhesion between matrix and fille. Impact strength values were supported by the results of SEM. From water adsorption test, composite with chemical modification showed low values as compared without modification indicating that modification has lowered the polarity of OPEFB.

EKSTRAKSI ACETOGENIN DARI DAUN DAN BIJI SIRSAK (Annona muricata L) DENGAN PELARUT ASETON Siswarni MZ, Nurhayani, Suci Damayanti Sinaga
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

Annona muricata L contain bioactive compounds acetogenins. Acetogenins which was synthesized through reaction between polyketide derived-acetic acid with 35-39 carbon atom in fatty acid, is the secondary metabolite of Annonaceae plant. This research aims to determine the variable that influence in leaf and Annona muricata seed extraction so that high yield value can be obtained and to prove the presence of acetogenins compound qualitatively. The materials used are Annona muricata leaves, Annona muricata seeds and aceton. The changing variables in this research is the mass of the samples for Annona muricata leaves powder that are 15 g, 25 g, 35 g and Annona muricata seeds powder that are 10 g, 20 g, 30 g which the extraction time are 30 minutes, 40 minutes, 50 minutes and 60 minutes. This research divided into two steps. The first step is the extraction of Annona muricata leaves and Annona muricata seeds using soxhletation method with 250 mL acetone for Annona muricata leaves, 200 mL aceton for Annona muricata seeds and extraction temperature is ± 58 oC. The second step is purification of the extract using distillation process. In this research, the highest yield value extract of Annona muricata leaves obtained is 55,33% with 15g mass of sample and 60 minutes for the extraction time. The highest yield value extract of Annona muricata seeds obtained is 62 % with 10 g mass of sample and 40 minutes for the extraction time. FTIR analysis showed the presence of functional groups such as lactone, THF, hyrdroxyl and aliphatic chains which indicates acetogenins compound’s presence.

PENGARUH WAKTU FERMENTASI TERHADAP VOLUME GAS BIO DAN PENYISIHAN COD DENGAN METODE PERLAKUANAWAL MENGGUNAKAN KALIUMHIDROKSIDA(KOH) PADA ECENG GONDOK (Eichhornia crassipes) Setiaty Pandia, Amin Trisnawati
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

The purpose of this study was to determine the effect of alkali pre-treatment methods on the quality and quantity of biogas. The study was doneby fermentation process the water hyacinth with KOH in a concentration of 6,7 M; 4 M;3 M; and 2,95 (M) with water in ratio hyacinth: water 70:30; 50:50; 30:70 and 100:0 (v/v) mixed with cow dung starter in an anaerobic digester batch system of 2,5 L capacity. In this study the highest biogas production at KOH concentration 4 M was in ratio of 50:50 (v/v)with yield biogas volume 449 mL and 86,52% of COD revomal, 92,42% of TSS removal. The lowest biogas production at KOH concentration 6,7 M was in ratio of 70:30 (v/v) with yield biogas volume 132 mL and 86,55% of COD removal and 88,65%of TSS removal.

ISOLASI PROTEIN SELAMA PROSES PENGAMBILAN KITIN DARI KULIT UDANG Kherliyanda Febriani, Fitri Hariani Nurza, Iriany
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jutek.v5i2.13699

Shrimp is one of the Indonesia fishery commodities with high economic value. The production of shrimp shells is usually 40-45% from crude shrimp. Shrimp shell contain protein, chitin, minerals and carotenoids. It is very potential to be used as materials for isolation of protein.This experiment is to determine factors that effect protein recovery and optimize deproteination processconditions to produce high yield of protein. The design of experiment used response surface methodology. It is 2 steps consist of deproteination and protein extraction process using shrimp shells and KOH solution in comparison 1:10 (w/v). The concentration of KOH are1,3 M; 2 M; 3 M; 4 M; 4,7 M. The reaction temperatures are37 oC; 40 oC; 45 oC; 50 oC; 53 oCand the reaction times are 40 minutes, 60 minutes, 90 minutes, 120 minutes, 140 minutes. Reaction temperature is the main factor influence protein recovery process. The highest protein yield obtained is 64,5826 % with protein content is 86,24% using KOH solution 2,98 M, reaction temperature 45,76 ºC and reaction time 90,51 minute. Economic potential by protein recovery during isolation of chitin from shrimp shells is profitable.

EKSTRAKSI MINYAK DARI BIJI KURMA (Phoenix dactylifera L.) DENGAN METODE SOXHLET EXTRACTION DENGAN MENGGUNAKAN ETIL ASETAT Taslim, Muhammad Rizky Agung, Sigit Purwanto
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jutek.v5i2.13721

Date palm seed is one of the waste by-products generated from industrial commodities. Date seed oil can be obtained through solvent extraction using a Soxhlet apparatus. In this experiment, date palm seed was used as raw material with ethyl acetate as the solvent. The experiment was carried out by varying extraction time and the mass ratio of date palm seed to solvent. The highest oil concentration of 9.5% was obtained at date palm seed to solvent mass ratio of 1:6 with extraction time of 2 hours. Peroxide value, iodine value, specific gravity, and free fatty acid content of date seed oil were, consecutively, 0.81 meq/kg oil, 10.15 mg/g, 0.80, and 0.52%. The highest fatty acid composition of date seed oil was oleic acid at 37.22% followed by lauric acid at 19.36%.

PENGARUH AGING PADA KEKUATAN TARIK (TENSILE STRENGTH) FILM LATEKS KARET ALAM BERPENGISI NANOKRISTALIN SELULOSA DAN PENYERASI ALKANOLAMIDA Marfuah Lubis; Nuim Hayat; Hamidah Harahap
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

Nanocrystalline cellulose is nano sized filler with high crystallinity and obtanained by hydrolysis of alpha cellulose from sugarcane bagasse. Tensile test of natural rubber latex film filled nanocrystalline cellulose and alkanolamide as compatibilizer after aging treatment have been done. Natural rubber latex films were prepared by coagulant dipping method and followed by vulcanization process at temperature 100 oC and 20 minutes. Aging treatment of natural rubber latex films have done at temperature 70 oC for 24 hours. Tensile test result of natural rubber latex filled nanocrystalline cellulose showed the tensile strength value of aged natural rubber latex film were lower than unaged one. However, tensile strength value of aged natural rubber latex film filled nanocrystalline cellulose modified alkanolamide were higher than unaged film.

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