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Hilda Yunita
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jurnal@rmpi.brin.go.id
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urania@brin.go.id
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Kawasan Sains dan Teknologi (KST) Bacharuddin Jusuf Habibie, Jl. Raya Puspiptek 60, Tangerang Selatan 15310
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Kota tangerang selatan,
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INDONESIA
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Published by BRIN Publishing
ISSN : 08524777     EISSN : 25280473     DOI : https://doi.org/10.55981/urania
Core Subject :
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir is a scientific publication platform that presents experimental research and development studies on the nuclear fuel cycle, covering radiation physics and chemistry, reactor engineering, nuclear safety and security, nuclear forensics, and radioactive waste management
Arjuna Subject : -
Articles 183 Documents
PENGARUH SERBUK U-Mo HASIL PROSES MEKANIK DAN HYDRIDE – DEHYDRIDE – GRINDING MILL TERHADAP KUALITAS PELAT ELEMEN BAKAR U-Mo/Al Supardjo Supardjo; Agoeng Kadarjono; Boybul Boybul
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 2 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.2.2260

Abstract

INFLUENCE OF U-Mo POWDER BY MECHANICAL AND HYDRIDE - DEHYDRIDE - GRINDING MILL PROCESS RESULT OF U-Mo / Al FUEL PLATE QUALITY. Research of U-7Mo/Al fuel type plate is done in order to develop U3Si2/Al fuel to get a new fuel that has a higher uranium density, stable for use as fuel in the reactor and is easily done if the reprocessed. The scope of the research includes manufacture: U-7Mo alloy with smelting techniques, pulverizing U-7Mo to be filed and hydride–dehydride–grinding mill, U-7Mo/Al fuel core with the technique of compacting at a pressure of 20 bar, and U-7Mo/Al fuel plate with technique of hot rolling at a temperature of 425oC. The U-7Mo alloy results smelting process quite homogeneous, the density of 16.34 g/cm3 and is tenacious, then made powder by means of filed and hydride–dehydride–grinding mill. The U-7Mo powder shaped flat results miserly process, contaminants Fe is high enough, whereas powder process results hydride- dehydride-grinding mill, tend equiaxial with low contaminants. The second type of U-7Mo powder is used as a raw material for making U-7Mo/Al fuel core and U-7Mo/Al fuel plate with 7 gU/cm3 uranium density and obtained product with almost the same quality. The U-7Mo/Al fuel core test results measuring 25 x 15 x 3.15 ± 0.05 mm, there is no defect/crack, U-7Mo distribution in the matrix is quite homogeneous and there is no grouping/agglomeration U-7Mo dimension >1 mm. The U-7Mo/Al fuel plate outcome rolling with a final thickness of 1.45 mm, has a thickness of 0.60 mm and a mean meat cladding thickness of 0.4 mm, and there is one point of measurement of cladding with a thickness of 0.15 mm. By comparing the use of both types of U-7Mo powders the U-7Mo/Al fuel core and U-7Mo/Al fuel plate produced has almost the same quality. However, the use of U-7Mo powder results hydride– dehydride–grinding mill process is better because the workmanship is faster and impurities in the powders can be minimized.
EFFECT OF Nb ELEMENT CONTENT IN U-Zr ALLOY ON HARDNESS, MICROSTRUCTURE AND PHASE FORMATION Masrukan Masrukan; M. Husna Al Hasa; Jan Setiawan; Slamet Pribadi
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 2 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.2.2261

Abstract

EFFECT OF Nb ELEMENT CONTENT IN U-Zr-Nb ALLOY ON HARDNESS, MICROSTRUCTURE AND PHASE FORMATION. Experiments to determine the effect of Nb element in the U-Zr alloys on hardness, microstructure and phase formation has been done. The addition of Nb element would effect the hardness, microstructure and phase which formed. The U-Zr-Nb alloy was made with the variation of Nb 2%, 5% and 8% by melting in an electric arc melting furnace that equipped with water cooling and the argon atmosphere. The U-Zr-Nb alloy to be cut divided to some testing, such as hardness test, microstructure, and phase analysis. Hardness testing was done by Vickers hardness testing equipment, microstructure by an optical microscope, and diffraction pattern by XRD and phase analysis was done by GSAS. Hardness testing results showed that the addition of 2% to 5% Nb element in U-Zr alloys will increased in hardness, but the addition of Nb element over 5% the hardness was decreased. Observations the microstructure showed that the addition of 2% to 5%Nb element, grains were formed from fine into coarse. Phase analysis for diffraction pattern showed that the phase changed from αU and γU (Zr,Nb)at 2% Nb to be αU, γU (Zr,Nb) and δ1 (UZr2) phase at 5% and 8% Nb. Phase changes was followed by changes in its compositions. The composition of αU at 2% Nb was 40% increased to 81% at 5% Nb and decreased to 3.9% at 8% Nb. The composition of γU decreased from 59,86% to 14,91% with increased Nb from 2% to 5% and further increased to 52,74% at 8% Nb.
KARAKTERISTIK MIKROSTRUKTUR DAN FASA PADUAN Zr- 0,3%Nb-0,5%Fe-0,5%Cr PASCA PERLAKUAN PANAS DAN PENGEROLAN DINGIN Sungkono Sungkono
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 2 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.2.2262

Abstract

MICROSTRUCTURE AND PHASE CHARACTERISTICSOF Zr-0.3%Nb-0.5%Fe-0.5%Cr ALLOY POST HEAT TREATMENT AND COLD ROLLING. Zr-Nb-Fe-Cr alloys was developed as fuel elements cladding with high burn up for advanced power reactors. In this research has been made of Zr-0.3% Nb-0.5% Fe-0.5% Cr alloy were heat treated with varying temperatures at650 and 750°C for 1 until 2 hours. The objectives of this research was to obtain the character of Zr-0.3% Nb-0.5% Fe-0.5% Cr alloy post heat treatment and cold rolling, microstructure nomenclature, crystal structure and phases that presents in the alloy. The results of this experiment showed that the microstructures of Zr-0.3% Nb-0.5% Fe-0.5% Cr alloy post heat treatment (650ºC, 1-2 hours) had equiaxial grain structure with an enlarged size with increasing of the retention time. Meanwhile, post heat treatment (750°C, 1-2 hours) occurred the microstructures evolution of alloy from equiaxial and columnar became equiaxial and columnar relatively large, and subsequently became the larger equiaxial grains. Zr-0.3% Nb-0.5% Fe-0.5% Cr alloy post heat treatment (650°C, 2 h) and (750°C, 1.5-2 hours) can undergo cold deformation without cracking when thickness reduction between 5 to 10%.The phases formation of Zr2Fe, ZrCr2 and FeCr compounds can improve the mechanical strength and the corrosion resistance of Zr-0.3% Nb-0.5% Fe-0.5% Cr alloy.
KETAHANAN KOROSI PADUAN Al-Mg 5052 DI DALAM AIR PENDINGIN NETRAL MENGANDUNG KLORIDA Dicky Tri Jatmiko; Isdiriayani Nurdin; Hary Devianto
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 2 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.2.2263

Abstract

CORROSION RESISTANCE OF Al-Mg ALLOY 5052 IN CHLORIDE CONTAINING NEUTRAL COOLING WATER. Al-Mg alloy 5052 is a material used as nuclear fuel element cladding due to its low neutron flux absorption and high corrosion resistance in demineralized water. This research is focused to know of the corrosion resistance of Al-Mg alloy 5052 in chloride containing neutral water used as demineralized primary cooling water substitute in GA Siwabessy Multi Purpose Reactor (RSG-GAS). This research covers the corrosion rate measurement using the Tafel method, corrosion process prediction using cyclic voltammetry method and corrosion product analysis using X-Ray Diffraction method. The experiments are carried out at temperature variation of 30°C, 35°C, 40°C and 45°C, as well as sodium chloride concentration of 0.05 M, 0.25 M and 0.5 M. The research results show that Al-Mg alloy 5052 is insignificantly to moderate corroded in chloride containing water by single step irreversible oxidation reaction.
OPTIMASI PENGGUNAAN HCl SEBAGAI LARUTAN PENGELUSI ITRIUM-90 DALAM DOWEX® 50WX8-200 Sulaiman Sulaiman; Sri Aguswarini; Karyad Karyad; Chairuman Chairuman; Gatot S; M Subur; Adang H G
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 2 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.2.2264

Abstract

OPTIMIZATION OF USE HCl AS SOLUTION FOR ELUTION ITRIUM-90 IN DOWEX® 50WX8- 200. Yttrium-90 is a β emitter radionuclide with a half life of 64.1 hours and emits the maximum β energy at 2280 keV. Yttrium-90 radionuclide is widely used in nuclear medicine for therapeutic purposes. 90Sr/90Y generator system has been developed to obtain carrier-free 90Y. Yttrium-90 were obtained from the 90Sr/90Y generator in the form of 90Y-citrate radiochemical. The 90Y ideal for tagging ligands is in the form of 90YCl3. To obtain the desired radiochemical a series of processes with ion exchange resin method is performed using Dowex® 50WX8-200. In this study optimization of the use of HCl for has been carried out 90Y elution from the resin with varied HCl concentration and contact time when 90Y is eluted from the resin. The release of 90Y from resin Dowex® 50WX8-200 depending on the concentration of HCl is used. The greater the concentration of HCl release rate of 90Y from 90Y-Dowex greater. The optimum contact time with 5 mL of 12 N HCl is 60 minutes with a result of 9.4%. The 90Y test results after eluted from Dowex® 50WX8-200 indicated that the 90Y was in the form of 90YCl3.
PEMBUATAN SERBUK U-6Zr DENGAN PENGKAYAAN URANIUM 19,75 % UNTUK BAHAN BAKAR REAKTOR RISET Masrukan Masrukan; Sungkono Sungkono; Yanlinastuti Yanlinastuti; Tri Yulianto; Ridwan Ridwan
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 3 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.3.2460

Abstract

Making U-6Zr alloy powder with enrichment of 19.75 % for a research reactor fuel has been done. Making of U-6Zr fuel in order to find new fuels that have a high density to replace the existing fuel U3Si2-Al. The purpose of this experiment was to determine the properties of U-6Zr alloy powder obtained from the hydriding-dehydriding process as a candidate research reactor fuel. Initially was made U-6Zr ingot by melting U and Zr metals using electric arc melting furnace. U-6Zr ingots were found then cut into pieces and put into hydriding-dehydriding equipment that operates at pressures 14,46054 psi and hydriding temperatures of 350 oC. Ingots that out of the hydriding-dehydriding equipment becomes brittle then was crushed so becomes powder. Powder that obtained subjected to the test, including chemical composition testing, density, hydrogen content, phase and thermal properties. The results testing show that chemical composition of some elements such as Al, Ca, Cu, and Ni exceeded the permitted limit, each of which contained elements of 202.21 ppm, 214.05 ppm, 61.25 ppm, and 134.53 ppm. On testing the density obtained that U-6Zr powder density of 13.57 g/cc and the testing of hydrogen residual content obtained hydrogen residual content of 0.16 %. For the testing phase were obtained the αU and δU phases, while in testing of the transformation temperature, there are two peaks, the first peak occurs at a temperature of 274 to 311 °C and a second peak occurs at a temperature of 493 to 527 oC. The first peak occurs endothermic reaction by absorbing heat of 6.23 cal/g but not formed a new phase, while the second peak occurs exothermic reaction with brought out heat of -9.34 cal/g and formed αZr phase. Meanwhile, the heat capacity of the test at temperature of 34 to 75 °C, the decrease in the value of the heat capacity accompanied heat absorption. At higher temperatures up to 437 °C, heat capacity value becomes negative and accompanied by heat expenditure. It can be concluded that the alloy the U-6Zr when viewed from the chemical composition can still be used for fuel research reactor. Residual hydrogen still found in small quantities in the U-6Zr powder that can be eliminated by heating for longer. Reaction between Zr with residual hydrogen to form the αZ phase is accompanied exothermic reaction with brought out heat of 93 449 cal/g.
PENGARUH PENGEROLAN PANAS TERHADAP KARAKTER PADUAN Zr-0,6Nb-0,5Fe-0,5Cr Sungkono Sungkono; Siti Aidah
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 3 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.3.2461

Abstract

Characters of Zr-0.6Nb-0.5Fe-0.5Cr alloy after hot rolling have been studied. The objective of this research was to obtain of hot rolling effect on the characteristics of microstructures, hardness and phases formed in Zr-0.6Nb-0.5Fe-0.5Cr  alloy. The hot rolling process of alloy carried out at temperature of  800 oC with retention time of 1.5 and 2 hours and a thickness reduction between 5 to 25 %. The results of this experiment showed that the Zr-0.6Nb-0.5Fe-0.5Cr alloy has Widmanstatten structure with microstructure evolving into deformed columnar grains and deformed elongated grains with increasing thickness reduction. Besides, the longer the retention time at temperature of 800 oC is the larger are the grain structures and formation of a-Zr and Zr3Fe phase. The hardness of  Zr-0.6Nb-0.5Fe-0.5Cr alloy has same trends i.e the larger thickness reduction gives higher hardness. The Zr-0.6Nb-0.5Fe-0.5Cr alloy can undergo hot rolling deformation at a thickness reduction of  25 %  and the formation of a-Zr and Zr3Fe can increased of hardness and strength of Zr-0.6 Nb-0.5 Fe-0.5 Cr alloy.
PENGARUH PEMANASAN KERNEL UO2 DALAM MEDIUM GAS ARGON TERHADAP SIFAT FISIS KERNEL UO2 SINTER Damunir Damunir; Sri Rinanti Susilowati; Ariyani Kusuma Dewi
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 3 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.3.2462

Abstract

The heating of UO2 kernels in argon gas medium on the physical properties of sinter UO2 kernels was conducted. The heated of the UO2 kernels was conducted in a sinter reactor of a bed type. The sample used was the UO2 kernels resulted from the reduction results at 800 oC temperature for 3 hours that had the density of 8.13 g/cm3; porosity of 0.26; O/U ratio of 2.05; diameter of 1146 µm and sphericity of 1.05. The sample was put into a sinter reactor, then it was vacuumed by flowing the argon gas at 180 mmHg pressure to drain the air from the reactor. After that, the cooling water and argon gas were continuously flowed with the pressure of 5 mPa with 1.5 liter/minutes velocity. The reactor temperature was increased and variated at 1200-1500 oC temperature and for 1-4 hours. The sinters UO2 kernels resulted from the study were analyzed in term of their physical properties including the density, porosity, diameter, sphericity, and specific surface area. The density was analyzed using pycnometer with CCl4 solution. The porosity was determined using Haynes equation. The diameters and sphericity were showed using the Dino-lite microscope. The specific surface area was determined using surface area meter Nova-1000. The obtained products showed tha the heating of UO2 kernel in argon gas medium were influenced on the physical properties of sinters UO2 kernel. The condition of best relatively at 1400 oC temperature and 2 hours time. The product resulted from the study was relatively at its best when heating was conducted at 1400 oC temperature and 2 hours time, produced sinters UO2 kernel with density of 10.14 gr/ml; porosity of 7 %; diameters of 893 µm; sphericity of 1.07 and specific surface area of 4.68 m2/g with solidify shrinkage of 22 %.
PEMBUATAN SUMBER RADIASI GAMMA 137Cs DENGAN AKTIVITAS 20 mCi DARI PEB U3Si2-Al PASCA IRADIASI DALAM CONTAINER STAINLESS STEEL Aslina Br Ginting; Yanlinastuti Yanlinastuti; Noviarty Noviarty; Boybul Boybul; Arif Nugroho; Dian Anggraini; Rosika Kriswarini; Sriyono Sriyono; Moch Subechi; Gatot Wurdiyanto; Hermawan Hermawan
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 3 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.3.2463

Abstract

In the post-irradiation examination of fuel element plate (PEB) U3Si2-Al), a solution of high activity as a result of testing nuclear fuel stored in hot cell with enough volume. The solution cannot be discarded as waste because it still contains fission isotope such as137Cs, uranium and trans uranium, which has a long half-life and dangerous for the environment. This can help the industry in order to fulfill the needs of a radioactive source in Indonesia, because until now 137Cs isotope is derived from foreign industries. In addition, the procurement and transportation of isotopes 137Cs require stringent requirements, because they have toget permission from the National Nuclear Energy Agency (BAPETEN), thus causing the price of high activity 137Cs isotopes becomes expensive to Indonesia. For these reasons, BATAN as nuclear R&D institutions in Indonesia need to study make isotopes 137Cs gamma radiation source, which is contained in the waste from spent fuel test results U3Si2-Al. Isotope 137Cs can be used very widely, such as in the analysis of environmental samples, the oil and gas industry, construction, radiography, fisheries, hospitals, and mining. Making isotope 137Cs gamma radiation source starting from the collection of waste from the test results PEB U3Si2- Al. Waste solution was collected in a bottle with volume 65 mL. Collection of 137Cs isotopes of other fission carried out using the method of cation exchange with weight 45 gr of zeolite Lampung. The results of separation are 137Cs-zeolite in the solid phase and the other isotopes are in the liquid phase. 137Cs-zeolite solid is then dried and then weighed and measured its activity using a spectrometer-g. Result of analysis by spectrometer-g was obtained activity of 137Cs-zeolite solids was 20 mCi.137Cs-zeolite solids then packed in sealed containers (shield source) capsule-shaped stainless steel and then certificate by PTKMR-BATAN.
PENENTUAN KANDUNGAN ISOTOP 235U DALAM PEB U3Si2-Al TMU 2,96 gU/cm3 UNTUK PERHITUNGAN BURN-UP Boybul Boybul; Yanlinastuti Yanlinastuti; Sutri Indaryati; Iis Haryati; Arif Nugroho
Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol. 21 No. 3 (2015): Urania: Jurnal Ilmiah Daur Bahan Bakar Nuklir
Publisher : Badan Riset dan Inovasi Nasional

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/urania.2015.21.3.2464

Abstract

235U separation has been carried out in the solution of PEB U3Si2 - Al with loading of uranium (TMU) 2.96 gU/cm3 at the Top. Top of PEB U3Si2-Al cut into three sections (triplo) with code T1, T2 and T3. Weight of each PEB code T1 = 0.095 g, T2 = 0.086 g and T3 = 0.087 g and dissolved using HCl and HNO3 in hotcell. The purpose of this study was to determine the content of the isotope 235U in the solution PEB U3Si2-Al post-irradiation and subsequently used for the calculation of burn-up. 235U isotope separation in the solution PEB U3Si2 - Al was conducted using an anion exchange column method using Dowex1x8 resin. Pipette solution of 100 mL, and then put into a column containing Dowex resin with a weight of 1.2 g. U effluent results in the column was eluted using 0.1 M HCl, then dried and conducted electro-deposition process and then analyzed using a spectrometer-α. The analysis showed that the content of the isotope 235U obtained at T1 = 0.03665 g/g PEB, T2 = 0.003468 g/g PEB and T3 = 0.03208 g/g PEB with separation recovery of 63.71 %. The content of isotope 235U obtained is used for the calculation of burn-up. burn-up calculation results of PEB U3Si2-Al of Top section (T1, T2 and T3) were obtained respectively by 43.31 %, 49.48 % and 45.41 % or burn-up an average of 45.75 %. This data is smaller than a data burn-up of PEB U3Si2-Al of middle section of 50.69 % conducted by previous researchers. However, this data can not be used as an input to the reactor, due to should be equipped with a data burn-up of PEB U3Si2-Al of bottom section. Therefore, in the nextstudies will be conducted calculation of burn-up PEB U3Si2-Al of bottom section.

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