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All Journal Jurnal Bahan Alam Terbarukan JURNAL KESEHATAN LINGKUNGAN (Journal of Environmental Health) Konversi ASEAN Journal of Chemical Engineering
Khoiroh, Ianatul
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Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Education Materials Science & Nanotechnology Public Health

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Isopropyl Alcohol Purification through Extractive Distillation using Glycerol as an Entrainer: Technical Performances Simulation and Design Hartanto, Dhoni; Handayani, Prima Astuti; Sutrisno, Akhmad; Anugrahani, Viona Widya; Mustain, Asalil; Khoiroh, Ianatul
Jurnal Bahan Alam Terbarukan Vol 8, No 2 (2019): December 2019 [Nationally Accredited - Sinta 2]
Publisher : Universitas Negeri Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15294/jbat.v8i2.23477

Abstract

Isopropyl alcohol is widely used as industrial chemical intermediates and common solvents in households, pharmaceuticals, food, cosmetics, and medical purposes. The high purity of isopropyl alcohol requires special separation from its impurity i.e. water due to isopropyl alcohol and water form an azeotropic point, which is difficult to separate using a conventional distillation method. The azeotropic point of this mixture is at isopropyl alcohol mole fraction of 0.68 and temperature of 353.4 K. One of the optimum methods to separate an azeotrope point is through the extractive distillation which use a third component as a solvent. Glycerol is one of the solvents which can be used as a potential entrainer in the extractive distillation. Glycerol is produced in the biodiesel production as a by-product. Moreover, glycerol is an eco-friendly chemical. In this work, the simulation of the extractive distillation of isopropyl alcohol/water system with glycerol as an entrainer was simulated using Aspen Plus. The Non-Random Two-Liquid (NRTL) model was used as thermodynamic model in the simulation.  The effect of stage number, binary feed stage, entrainer feed stage, and reflux ratio to the purity of isopropyl alcohol, and reboiler-condenser duties were examined to achieve the optimum design for the extractive distillation column with less energy requirements. The simulation results showed that the optimum configurations in the extractive distillation column design are at 25 theoretical stages, binary feed stage (BFS) of 20, entrainer feed stage (EFS) of 2, and reflux ratio (RR) of 0.5 to produce isopropyl alcohol with the purity of 99.27%. The design and sizing of the extractive distillation column were also proposed in this work.
Effect of long chain fatty acids on biogas production and biochemical kinetics in anaerobic bioreactors: a review Kahar, Abdul; Khoiroh, Ianatul
Konversi Vol 13, No 1 (2024): April 2024
Publisher : Universitas Lambung Mangkurat

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20527/k.v13i1.19035

Abstract

Long Chain Fatty Acids (LCFAs) are the primary intermediate byproduct of the lipid (fats, oils, and greases) degradation process, and if they accumulate in high concentrations, they can cause failure or reduce the performance of anaerobic bioreactors due to sludge flotation issues, biochemical kinetics problems for soluble substrates, inhibition of microbial activity, and inefficient biogas recovery. Understanding the biochemical kinetics of anaerobic bioreactors requires taking into account the entire process, including microbe growth, substrate degradation, and product synthesis. Biochemical kinetics of anaerobic treatment is the study of polymer biodegradation rates of insoluble organic matter in wastewater, which is the mechanism of bond breaking and bond formation in biochemical reactions. As a result, biochemical kinetics allow for the design of both desired and undesirable reaction phases. The kinetic parameters acquired are utilized to design, operate, and optimize anaerobic bioreactors for wastewater treatment on a technical scale.
Extractive Distillation of Ethanol/Water with 1-Butyl-3-Methylimidazolium Bromide Ionic Liquid as a Separating Agent: Process Simulation Hartanto, Dhoni; Handayani, Prima Astuti; Astuti, Widi; Kusumaningtyas, Ratna Dewi; Purwana, Yulian Candra; Maftukhaturrizqiyah, Maftukhaturrizqiyah; Wijayanti, Reni Titis; Wulansari, Durroti Zuhriah; Wulansarie, Ria; Pradnya, Irene Nindita; Hadikawuryan, Danang Subarkah; Wibowo, Agung Ari; Sholihin, Riza Mazidu; Chafidz, Achmad; Khoiroh, Ianatul
ASEAN Journal of Chemical Engineering Vol 23, No 3 (2023)
Publisher : Department of Chemical Engineering, Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ajche.72250

Abstract

Ethanol purification has become of great interest recently because ethanol can be used as renewable energy, solvent in many industries, and for medicinal purposes. The separation of ethanol from water is challenging because the azeotropic point has appeared in this binary mixture. Extractive distillation technology is one of the most interesting methods to separate ethanol from water due to the competitiveness of its energy consumption and capital investment costs. Ionic liquids such as 1-butyl-3-methylimidazolium bromide [BMIM] [Br], categorized as a green solvent, produce a significant salting-out effect in the ethanol-water system. This makes ionic liquid a promising solvent in ethanol-water separation. This study simulated the extractive distillation of an ethanol-water system with 1-butyl-3-methylimidazolium bromide as a solvent. The simulation and sensitivity analysis were performed on the Aspen Plus Process Simulator to obtain the optimum configuration. The NRTL thermodynamic model was used in this study. The effects of the number of stages (NS), binary feed stage (BFS), entrainer feed stage (EFS), and reflux ratio (RR) on the ethanol concentration with minimum energy requirements were studied. The most optimal configurations to produce a high ethanol concentration with less energy are NS 28, BFS 22, EFS 4, and RR 1.5.
Coconut Shells, Water Hyacinth and Rice Husks are Very Effective in Improving the Quality of Physical and Chemical Standards of Dug Well Water in Flood Areas Marlinae, Lenie; Biyatmoko, Danang; Husaini; Irawan, Chairul; Arifin, Syamsul; R Saidi, Akhmad; Fithria, Abdi; Zubaidah, Tien; M. Ratodi; A. Mourad, Khaldoon; Khairiyati, Laily; Waskito, Agung; H.D Lasari, Hadrianti; Khoiroh, Ianatul
JURNAL KESEHATAN LINGKUNGAN Vol. 16 No. 3 (2024): JURNAL KESEHATAN LINGKUNGAN
Publisher : Universitas Airlangga

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20473/jkl.v16i3.2024.255-265

Abstract

Introduction: Ensuring access to clean and safe drinking water is crucial, especially in flood-prone regions where the water quality in dug wells can deteriorate due to various physicochemical factors. This research was aimed to measure the effectiveness of natural materials in improving water quality based on physicochemical parameters and to compare water quality before and after treatment in Astambul Subdistrict of Banjar Regency, South Kalimantan Province. Methods: The study involved a survey of 192 private boreholes and dug wells across five villages in the Astambul Subdistrict, with 30 samples selected for detailed analysis. Key physicochemical parameters analyzed included total dissolved solids (TDS), dissolved oxygen (DO), turbidity, and total suspended solids (TSS). TDS, with a standard limit of 50 mg/L, served as a primary water quality indicator. DO, essential for gauging water oxygenation, and was measured as it results from photosynthesis and atmospheric absorption. Turbidity was assessed using a turbidimeter to determine water clarity, and a UV-vis Spectrophotometer 2008 was utilized to measure levels of iron (Fe) and mangasene (Mn). Results and Discussion: The findings demonstrated that coconut shells, husks, and water hyacinths improved water quality across physical and chemical parameters. Statistical analysis using t-tests showed improvements in these parameters after treatment. For example, DO levels increased in multiple villages, with the highest percentage in Kaliukan Village (59.2%) and decreases in turbidity and TSS. Conclusion: The study concluded that coconut shells, husks, and water hyacinths have potential to enhance physicochemical quality of water.
Co-Authors A. Mourad, Khaldoon Abdi Fithria Abdul Kahar Agung Ari Wibowo Anugrahani, Viona Widya Asalil Mustain Chafidz, Achmad Chairul Irawan Danang Biyatmoko, Danang Dhoni Hartanto H.D Lasari, Hadrianti Hadikawuryan, Danang Subarkah Husaini Laily Khairiyati Lenie Marlinae M. Ratodi Maftukhaturrizqiyah, Maftukhaturrizqiyah Pradnya, Irene Nindita Prima Astuti Handayani Purwana, Yulian Candra R Saidi, Akhmad Ratna Dewi Kusumaningtyas Ria Wulansarie, Ria Riza Mazidu Sholihin Sutrisno, Akhmad Syamsul Arifin Waskito, Agung Widi Astuti Wijayanti, Reni Titis Wulansari, Durroti Zuhriah