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All Journal Jurnal Fisika Unand Chemistry Indonesian Journal of Chemical Research
Lubis, Muhammad Frassetia
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Biochemistry, Genetics & Molecular Biology Chemistry Earth & Planetary Sciences Electrical & Electronics Engineering Energy Engineering Environmental Science Materials Science & Nanotechnology Physics

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Synthesis, Microstructure, Optical Properties, and Sensitive Amoxicillin Detection of Carbon Dots Lubis, Yuni Aldriani; Gea, Saharman; Lubis, Muhammad Frassetia; Pai, Woei Wu Larry; Marpongahtun, Marpongahtun
Indonesian Journal of Chemical Research Vol 13 No 1 (2025): Edition for May 2025
Publisher : Jurusan Kimia, Fakultas Sains dan Teknologi, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598/ijcr.2025.13-yun

Abstract

The detection of amoxicillin has been successfully carried out using C-dot fluorescence probes made from d-glucose and urea. The fluorescence probe has an intense bright blue emission under UV light at 395 nm and and depends on the excitation and depends on the excitation. Raman studies successfully showed a D peak at 1381 cm-1 and a G peak at 1586 cm-1 associated with graphitic and amorphous structures. The absorption peaks in UV-vis spectroscopy confirm transitions at 275 nm (π → π*) and 322 nm (n → π*) with the presence of conjugated C=C and carbonyl (C=O) functional groups. The results of the fluorescence test show a bright blue color, with its intensity measured at an excitation of 365 nm. This can be attributed to nitrogen incorporation on the surface of the C-dots derived from urea, resulting in a quantum yield of 54%. This fluorescence probe is highly sensitive in detecting amoxicillin, as evidenced by the successful detection of AMX at concentrations of 10–30 μM and a resulting LOD of 5.75443×10−7 nM. The microstructure shows a uniform size of C-dot nanoparticles, and C-dot modeling was created. C-dot probes have an LOD of 5.75443×10−7 nM, indicating high sensitivity in detecting AMX.
Sintesis Lapisan Antikorosi Menggunakan Tanin dari Kulit Batang Bakau sebagai Inhibitor Lubis, Muhammad Frassetia; Dahlan, Dahyunir
Jurnal Fisika Unand Vol 9 No 2 (2020)
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jfu.9.2.277-283.2020

Abstract

Telah disintesis lapisan antikorosi menggunakan tanin dari kulit batang bakau sebagai inhibitor. Lapisan dibuat dari campuran tembaga (II) sulfat 1 M, asam borat 0,24 M dan akuabides tanpa dan dengan ekstrak kulit batang bakau pada konsentrasi 0%; 0,5%; 1%; 1,5%; 2%; 2,5% dan 3% volume dengan metode elektrodeposisi. Larutan NaOH 1 M digunakan sebagai media pengkorosi selama 4,5 jam. Karakterisasi morfologi dilakukan pada sampel terbaik dengan X-Ray Difractometer (XRD) setelah elektrodeposisi dengan 2,5% volume inhibitor baik sebelum maupun setelah dilakukan pengukuran laju korosi. Perubahan tegangan setelah elektrodeposisi adalah sebesar 0,1 V untuk semua variasi inhibitor. Laju korosi dan efisiensi inhibisi memiliki perubahan signifikan pada 2,5% volume inhibitor. Karakterisasi dengan mikroskop digital memiliki hasil optimum pada pelat baja dengan 2% inhibitor. Anticorrosion layers have been synthesized using tannins from mangrove bark as inhibitors. The coating was made from a mixture of 1 M copper (II) sulfate, 0.24 M boric acid and aquabides without and with mangrove bark extract at a concentration of 0%; 0.5%; 1%; 1.5%; 2%; 2.5% and 3% volume by electrodeposition method. 1 M NaOH solution was used as a corroding medium for 4.5 hours. Morphological characterization was performed on the best samples with X-Ray Difractometer (XRD) after electrodeposition with 2.5% volume inhibitors both before and after corrosion rate measurements. The change in voltage after electrodeposition is 0.1 V for all variations of the inhibitor. Corrosion rate and inhibition efficiency have a significant change in 2.5% volume inhibitors. Characterization with a digital microscope has optimum results on steel plates with 2% inhibitors.
Co-Authors Dahyunir Dahlan Lubis, Yuni Aldriani Marpongahtun, Marpongahtun Pai, Woei Wu Larry Saharman Gea